N-(2-(1H-indol-3-yl)ethyl)-3-trifluoroacetamidobenzamide

Base Information

Chemical Name:N-(2-(1H-indol-3-yl)ethyl)-3-trifluoroacetamidobenzamide
CAS No.:1616559-70-6
Molecular Formula:C₁₉H₁₆F₃N₃O₂
Molecular Weight:375.35
Hs Code.:

Synonyms:N-(2-(1H-indol-3-yl)ethyl)-3-trifluoroacetamidobenzamide

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Chemical Property of N-(2-(1H-indol-3-yl)ethyl)-3-trifluoroacetamidobenzamide

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Technology Process of N-(2-(1H-indol-3-yl)ethyl)-3-trifluoroacetamidobenzamide

There total 3 articles about N-(2-(1H-indol-3-yl)ethyl)-3-trifluoroacetamidobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 33284-01-4
N-(2-(1H-indol-3-yl)ethyl)-3-aminobenzamide

: 76-05-1
trifluoroacetic acid

: 1616559-70-6
N-(2-(1H-indol-3-yl)ethyl)-3-trifluoroacetamidobenzamide

Guidance literature:: trifluoroacetic acid; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 0.5h;

N-(2-(1H-indol-3-yl)ethyl)-3-aminobenzamide; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1021/ml500131a

Reference yield:

: 61-54-1
tryptamine

: 1616559-70-6
N-(2-(1H-indol-3-yl)ethyl)-3-trifluoroacetamidobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 20 °C

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / 20 °C

2.2: 24 h / 20 °C

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ml500131a

Reference yield:

: 99-05-8,159139-79-4
meta-aminobenzoic acid

: 1616559-70-6
N-(2-(1H-indol-3-yl)ethyl)-3-trifluoroacetamidobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 20 °C

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / 20 °C

2.2: 24 h / 20 °C

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ml500131a