Technology Process of C15H14N2O
There total 6 articles about C15H14N2O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
methanesulfonyl chloride; triethylamine;
In
dichloromethane;
at 0 - 20 ℃;
DOI:10.1016/j.bmcl.2011.05.052
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium tetrahydroborate / methanol / 4 h / 20 °C
2: methanesulfonyl chloride; triethylamine / dichloromethane / 0 - 20 °C
With
sodium tetrahydroborate; methanesulfonyl chloride; triethylamine;
In
methanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.05.052
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: triethylamine / acetonitrile / 20 °C
2.1: sodium hydroxide
2.2: 20 °C
3.1: phosphorus pentoxide
4.1: potassium carbonate / acetonitrile / 8 h / Reflux
5.1: sodium tetrahydroborate / methanol / 4 h / 20 °C
6.1: methanesulfonyl chloride; triethylamine / dichloromethane / 0 - 20 °C
With
sodium tetrahydroborate; phosphorus pentoxide; potassium carbonate; methanesulfonyl chloride; triethylamine; sodium hydroxide;
In
methanol; dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2011.05.052