3.7-Dimethyl-1t-(2.2.6-trimethyl-cyclohexadien-(4.6)-yl)-nonatetraen-(1.3c.5t.7t)-ol-(9)

Base Information

Chemical Name:3.7-Dimethyl-1t-(2.2.6-trimethyl-cyclohexadien-(4.6)-yl)-nonatetraen-(1.3c.5t.7t)-ol-(9)
CAS No.:73285-25-3
Molecular Formula:C₂₀H₂₈O
Molecular Weight:284.442
Hs Code.:

3.7-Dimethyl-1<i>t</i>-(2.2.6-trimethyl-cyclohexadien-(4.6)-yl)-nonatetraen-(1.3<i>c</i>.5<i>t</i>.7<i>t</i>)-ol-(9)

Synonyms:3.7-Dimethyl-1t-(2.2.6-trimethyl-cyclohexadien-(4.6)-yl)-nonatetraen-(1.3c.5t.7t)-ol-(9)

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Chemical Property of 3.7-Dimethyl-1t-(2.2.6-trimethyl-cyclohexadien-(4.6)-yl)-nonatetraen-(1.3c.5t.7t)-ol-(9)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 3.7-Dimethyl-1t-(2.2.6-trimethyl-cyclohexadien-(4.6)-yl)-nonatetraen-(1.3c.5t.7t)-ol-(9)

There total 9 articles about 3.7-Dimethyl-1t-(2.2.6-trimethyl-cyclohexadien-(4.6)-yl)-nonatetraen-(1.3c.5t.7t)-ol-(9) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79-80-1,58865-03-5,73285-25-3,83945-89-5,90694-28-3,90694-29-4,93380-03-1,93381-02-3
Vitamin A₂

Guidance literature:: Belonesox belizamis;
DOI:10.1038/2061161a0

Reference yield:

: 14398-42-6
(2E,4E)-3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienoic acid

: 73285-25-3
3.7-Dimethyl-1t-(2.2.6-trimethyl-cyclohexadien-(4.6)-yl)-nonatetraen-(1.3c.5t.7t)-ol-(9)

Guidance literature:: Multi-step reaction with 8 steps

1: K₂CO₃

2: (i) NBS, CaO, NaHCO₃, (ii) quinoline, (iii) KOH, MeOH

3: LiAlH₄

4: MnO₂

5: (i) NaNH₂, (ii) KOH, MeOH

6: I₂ / Irradiation

7: K₂CO₃

8: LiAlH₄

With manganese(IV) oxide; lithium aluminium tetrahydride; iodine; potassium carbonate;
DOI:10.1002/hlca.19620450216

Reference yield:

: 14538-58-0
3-methyl-5t-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-2t,4-dienoic acid methyl ester

: 73285-25-3
3.7-Dimethyl-1t-(2.2.6-trimethyl-cyclohexadien-(4.6)-yl)-nonatetraen-(1.3c.5t.7t)-ol-(9)

Guidance literature:: Multi-step reaction with 7 steps

1: (i) NBS, CaO, NaHCO₃, (ii) quinoline, (iii) KOH, MeOH

2: LiAlH₄

3: MnO₂

4: (i) NaNH₂, (ii) KOH, MeOH

5: I₂ / Irradiation

6: K₂CO₃

7: LiAlH₄

With manganese(IV) oxide; lithium aluminium tetrahydride; iodine; potassium carbonate;
DOI:10.1002/hlca.19620450216