3-bromo-4-methoxyphenylaminoketone hydrochloride

Base Information

Chemical Name:3-bromo-4-methoxyphenylaminoketone hydrochloride
CAS No.:1435972-35-2
Molecular Formula:C₉H₁₀BrNO₂*ClH
Molecular Weight:280.549
Hs Code.:

Synonyms:3-bromo-4-methoxyphenylaminoketone hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-bromo-4-methoxyphenylaminoketone hydrochloride

Chemical Property:

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Technology Process of 3-bromo-4-methoxyphenylaminoketone hydrochloride

There total 5 articles about 3-bromo-4-methoxyphenylaminoketone hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1435972-34-1
C₁₁H₁₀BrNO₄

: 1435972-35-2
3-bromo-4-methoxyphenylaminoketone hydrochloride

Guidance literature:: With hydrogenchloride; acetic acid; In water; Reflux;
DOI:10.1016/j.bmcl.2013.03.082

Reference yield:

: 6096-83-9
2?bromo?1?(3?bromo?4?methoxyphenyl)ethan?1?one

: 1435972-35-2
3-bromo-4-methoxyphenylaminoketone hydrochloride

Guidance literature:: 2?bromo?1?(3?bromo?4?methoxyphenyl)ethan?1?one; With hexamethylenetetramine; In chloroform; at 20 ℃; for 2h;

With hydrogenchloride; In ethanol; at 20 ℃; for 48h;
DOI:10.1016/j.ejmech.2019.01.057

Reference yield:

: 3114-09-8
3-bromo-4-methoxychloroacetophenone

: 1435972-35-2
3-bromo-4-methoxyphenylaminoketone hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 20 °C

2: hydrogenchloride; acetic acid / water / Reflux

With hydrogenchloride; acetic acid; In water; acetonitrile;
DOI:10.1016/j.bmcl.2013.03.082