1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7-methoxy-1H-2-benzazepin-hydrochlorid

Base Information

Chemical Name:1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7-methoxy-1H-2-benzazepin-hydrochlorid
CAS No.:115032-06-9
Molecular Formula:C₁₉H₂₃NO₃*ClH
Molecular Weight:349.857
Hs Code.:

Synonyms:1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7-methoxy-1H-2-benzazepin-hydrochlorid

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Chemical Property of 1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7-methoxy-1H-2-benzazepin-hydrochlorid

Chemical Property:

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Technology Process of 1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7-methoxy-1H-2-benzazepin-hydrochlorid

There total 5 articles about 1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7-methoxy-1H-2-benzazepin-hydrochlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 115032-13-8
1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7-methoxy-1H-2-benzazepin

: 115032-06-9
1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7-methoxy-1H-2-benzazepin-hydrochlorid

Guidance literature:: With hydrogenchloride; In diethyl ether; ethanol;

Reference yield:

: 18655-52-2
3-(3-methoxyphenyl)propan-1-amine

: 115032-06-9
1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7-methoxy-1H-2-benzazepin-hydrochlorid

Guidance literature:: Multi-step reaction with 4 steps

1: 64 percent / C₅H₅N / CHCl₃ / 1 h / Ambient temperature

2: 78 percent / POCl₃ / acetonitrile / 20 h / Heating

3: NaBH₄ / methanol / 0.5 h / Heating

4: 87 percent / HCl / ethanol; diethyl ether

With pyridine; hydrogenchloride; sodium tetrahydroborate; trichlorophosphate; In methanol; diethyl ether; ethanol; chloroform; acetonitrile;

Reference yield:

: 115031-99-7
3,4-Dimethoxy-N-<3-(3-methoxyphenyl)propyl>benzamid

: 115032-06-9
1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7-methoxy-1H-2-benzazepin-hydrochlorid

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / POCl₃ / acetonitrile / 20 h / Heating

2: NaBH₄ / methanol / 0.5 h / Heating

3: 87 percent / HCl / ethanol; diethyl ether

With hydrogenchloride; sodium tetrahydroborate; trichlorophosphate; In methanol; diethyl ether; ethanol; acetonitrile;