DL-2,3-bis{[3-(3,4-dimethoxyphenyl)acryloyl]amino}propionic acid methyl ester

Base Information

Chemical Name:DL-2,3-bis{[3-(3,4-dimethoxyphenyl)acryloyl]amino}propionic acid methyl ester
CAS No.:227098-01-3
Molecular Formula:C₂₆H₃₀N₂O₈
Molecular Weight:498.533
Hs Code.:

Synonyms:DL-2,3-bis{[3-(3,4-dimethoxyphenyl)acryloyl]amino}propionic acid methyl ester

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Chemical Property of DL-2,3-bis{[3-(3,4-dimethoxyphenyl)acryloyl]amino}propionic acid methyl ester

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Technology Process of DL-2,3-bis{[3-(3,4-dimethoxyphenyl)acryloyl]amino}propionic acid methyl ester

There total 1 articles about DL-2,3-bis{[3-(3,4-dimethoxyphenyl)acryloyl]amino}propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 14737-89-4
3,4-dimethoxy-trans-cinnamic acid

: 6059-44-5,106973-48-2,147857-43-0
methyl 2,3-diaminopropanoate dihydrochloride

: 227098-01-3
DL-2,3-bis{[3-(3,4-dimethoxyphenyl)acryloyl]amino}propionic acid methyl ester

Guidance literature:: With 4-methyl-morpholine; 1-hydroxybenzotriazol-hydrate; diisopropyl-carbodiimide; In dichloromethane; Ambient temperature;
DOI:10.1021/jm980531m

Reference yield: 99.0%

: 227098-01-3
DL-2,3-bis{[3-(3,4-dimethoxyphenyl)acryloyl]amino}propionic acid methyl ester

: 227098-04-6
DL-2,3-bis{[3-(3,4-dimethoxyphenyl)acryloyl]amino}propionic acid

Guidance literature:: With lithium hydroxide; In various solvents; for 8h;
DOI:10.1016/j.bmc.2006.02.030

Reference yield:

: 227098-01-3
DL-2,3-bis{[3-(3,4-dimethoxyphenyl)acryloyl]amino}propionic acid methyl ester

: 2,3-Bis-[(E)-3-(3,4-dimethoxy-phenyl)-acryloylamino]-propionic acid 2,2-dimethyl-propionyloxymethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / lithium hydroxide / various solvents / 8 h

2: triethylamine / dimethylformamide / 3 h / 70 °C

With lithium hydroxide; triethylamine; In various solvents; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2006.02.030