3-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-6-(phenylethynyl)pyridazine

Base Information

Chemical Name:3-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-6-(phenylethynyl)pyridazine
CAS No.:1234347-89-7
Molecular Formula:C₅₃H₄₇ClN₂O₅
Molecular Weight:827.42
Hs Code.:

Synonyms:3-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-6-(phenylethynyl)pyridazine

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Chemical Property of 3-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-6-(phenylethynyl)pyridazine

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Technology Process of 3-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-6-(phenylethynyl)pyridazine

There total 1 articles about 3-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-6-(phenylethynyl)pyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1234347-85-3
3-chloro-6-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)pyridazine

: 536-74-3
phenylacetylene

: 1234347-89-7
3-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-6-(phenylethynyl)pyridazine

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmcl.2010.04.006

Reference yield:

: 1234347-89-7
3-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-6-(phenylethynyl)pyridazine

: 108-24-7
acetic anhydride

: C₃₄H₃₃ClN₂O₈

Guidance literature:: 3-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-6-(phenylethynyl)pyridazine; acetic anhydride; With trimethylsilyl trifluoromethanesulfonate; at -30 - 20 ℃; for 15h; Inert atmosphere;

With water; sodium hydrogencarbonate;