2,5-Dihydro-3-<3-(4-fluoro-3-nitrophenyl)-3-oxo-1-propenyl>-2,2,5,5-tetramethyl-1H-pyrrol-1-yloxyl radical

Base Information

Chemical Name:2,5-Dihydro-3-<3-(4-fluoro-3-nitrophenyl)-3-oxo-1-propenyl>-2,2,5,5-tetramethyl-1H-pyrrol-1-yloxyl radical
CAS No.:124558-43-6
Molecular Formula:C₁₇H₁₈FN₂O₄
Molecular Weight:333.339
Hs Code.:

Synonyms:2,5-Dihydro-3-<3-(4-fluoro-3-nitrophenyl)-3-oxo-1-propenyl>-2,2,5,5-tetramethyl-1H-pyrrol-1-yloxyl radical

Suppliers and Price of 2,5-Dihydro-3-<3-(4-fluoro-3-nitrophenyl)-3-oxo-1-propenyl>-2,2,5,5-tetramethyl-1H-pyrrol-1-yloxyl radical

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,5-Dihydro-3-<3-(4-fluoro-3-nitrophenyl)-3-oxo-1-propenyl>-2,2,5,5-tetramethyl-1H-pyrrol-1-yloxyl radical

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,5-Dihydro-3-<3-(4-fluoro-3-nitrophenyl)-3-oxo-1-propenyl>-2,2,5,5-tetramethyl-1H-pyrrol-1-yloxyl radical

There total 3 articles about 2,5-Dihydro-3-<3-(4-fluoro-3-nitrophenyl)-3-oxo-1-propenyl>-2,2,5,5-tetramethyl-1H-pyrrol-1-yloxyl radical which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 124558-29-8
C₁₇H₁₉FNO₂

: 124558-43-6
2,5-Dihydro-3-<3-(4-fluoro-3-nitrophenyl)-3-oxo-1-propenyl>-2,2,5,5-tetramethyl-1H-pyrrol-1-yloxyl radical

Guidance literature:: With sulfuric acid; nitric acid; at 0 ℃; for 1h;
DOI:10.1055/s-1989-27306

Reference yield:

: 71051-83-7
3-formyl-2,2,5,5-tetramethyl-pyrroline-1-oxyl

: 124558-43-6
2,5-Dihydro-3-<3-(4-fluoro-3-nitrophenyl)-3-oxo-1-propenyl>-2,2,5,5-tetramethyl-1H-pyrrol-1-yloxyl radical

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / 10percent aq. NaOH / ethanol / 3 h / 25 °C

2: 52 percent / conc. H₂SO₄, 67percent HNO₃ / 1 h / 0 °C

With sodium hydroxide; sulfuric acid; nitric acid; In ethanol;
DOI:10.1055/s-1989-27306

Reference yield:

: 403-42-9
1-(4-fluorophenyl)ethanone

: 124558-43-6
2,5-Dihydro-3-<3-(4-fluoro-3-nitrophenyl)-3-oxo-1-propenyl>-2,2,5,5-tetramethyl-1H-pyrrol-1-yloxyl radical

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / 10percent aq. NaOH / ethanol / 3 h / 25 °C

2: 52 percent / conc. H₂SO₄, 67percent HNO₃ / 1 h / 0 °C

With sodium hydroxide; sulfuric acid; nitric acid; In ethanol;
DOI:10.1055/s-1989-27306