Technology Process of C18H14O2
There total 4 articles about C18H14O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium hydroxide monohydrate; water;
In
tetrahydrofuran;
at 20 ℃;
DOI:10.1021/jm301470a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / methanol / 1 h / 20 °C
2: di‐tert‐butyl‐(1‐phenylindol‐2‐yl)phosphane; copper(l) iodide; N,N,N,N,-tetramethylethylenediamine; sodium tetrachloropalladate(II) / water / 80 °C / Schlenk technique; Inert atmosphere
3: lithium hydroxide monohydrate; water / tetrahydrofuran / 20 °C
With
copper(l) iodide; sodium tetrachloropalladate(II); lithium hydroxide monohydrate; N,N,N,N,-tetramethylethylenediamine; water; potassium carbonate; di‐tert‐butyl‐(1‐phenylindol‐2‐yl)phosphane;
In
tetrahydrofuran; methanol; water;
2: |Sonogashira Cross-Coupling;
DOI:10.1021/jm301470a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: di‐tert‐butyl‐(1‐phenylindol‐2‐yl)phosphane; copper(l) iodide; N,N,N,N,-tetramethylethylenediamine; sodium tetrachloropalladate(II) / water / 80 °C / Schlenk technique; Inert atmosphere
2: lithium hydroxide monohydrate; water / tetrahydrofuran / 20 °C
With
copper(l) iodide; sodium tetrachloropalladate(II); lithium hydroxide monohydrate; N,N,N,N,-tetramethylethylenediamine; water; di‐tert‐butyl‐(1‐phenylindol‐2‐yl)phosphane;
In
tetrahydrofuran; water;
1: |Sonogashira Cross-Coupling;
DOI:10.1021/jm301470a
