(R)-2-O-acetoxymethyl-3-O-p-toluenesulfonyl-1-O-trimethylacetyl-1,2,3-propanetriol

Base Information

Chemical Name:(R)-2-O-acetoxymethyl-3-O-p-toluenesulfonyl-1-O-trimethylacetyl-1,2,3-propanetriol
CAS No.:141110-73-8
Molecular Formula:C₁₈H₂₆O₈S
Molecular Weight:402.466
Hs Code.:

Synonyms:(R)-2-O-acetoxymethyl-3-O-p-toluenesulfonyl-1-O-trimethylacetyl-1,2,3-propanetriol

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Chemical Property of (R)-2-O-acetoxymethyl-3-O-p-toluenesulfonyl-1-O-trimethylacetyl-1,2,3-propanetriol

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Technology Process of (R)-2-O-acetoxymethyl-3-O-p-toluenesulfonyl-1-O-trimethylacetyl-1,2,3-propanetriol

There total 6 articles about (R)-2-O-acetoxymethyl-3-O-p-toluenesulfonyl-1-O-trimethylacetyl-1,2,3-propanetriol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 108-24-7
acetic anhydride

: 141110-72-7
(R)-2-O-methoxymethyl-3-O-p-toluenesulfonyl-1-O-trimethylacetyl-1,2,3-propanetriol

: 141110-73-8
(R)-2-O-acetoxymethyl-3-O-p-toluenesulfonyl-1-O-trimethylacetyl-1,2,3-propanetriol

Guidance literature:: With boron trifluoride diethyl etherate; at 0 ℃; for 2h;
DOI:10.1135/cccc19931151

Reference yield:

: 4195-19-1
pivaloyl imidazole

: 141110-73-8
(R)-2-O-acetoxymethyl-3-O-p-toluenesulfonyl-1-O-trimethylacetyl-1,2,3-propanetriol

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / triethylamine / CH₂Cl₂ / 168 h / Ambient temperature

2: 88 percent / phosphorus oxychloride / CH₂Cl₂ / 0.5 h

3: 96 percent / boron trifluoride etherate / 2 h / 0 °C

With boron trifluoride diethyl etherate; triethylamine; trichlorophosphate; In dichloromethane;
DOI:10.1135/cccc19931151

Reference yield:

: 41274-09-3
(R)-3-tosyloxy-1,2-propanediol

: 141110-73-8
(R)-2-O-acetoxymethyl-3-O-p-toluenesulfonyl-1-O-trimethylacetyl-1,2,3-propanetriol

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / triethylamine / CH₂Cl₂ / 168 h / Ambient temperature

2: 88 percent / phosphorus oxychloride / CH₂Cl₂ / 0.5 h

3: 96 percent / boron trifluoride etherate / 2 h / 0 °C

With boron trifluoride diethyl etherate; triethylamine; trichlorophosphate; In dichloromethane;
DOI:10.1135/cccc19931151