Technology Process of beta-D-arabino-Hexopyranose, 4-amino-1,6-anhydro-2,4-dideoxy- (9CI)
There total 5 articles about beta-D-arabino-Hexopyranose, 4-amino-1,6-anhydro-2,4-dideoxy- (9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen; triethylamine;
palladium on activated charcoal;
In
ethyl acetate;
under 760 Torr;
DOI:10.1016/S0223-5234(00)00114-8
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 55 percent / NaN3; NH4Cl / methanol; H2O / 24 h / Heating
2: 81 percent / H2; Et3N / 10 percent Pd-C / ethyl acetate / 760 Torr
With
sodium azide; hydrogen; ammonium chloride; triethylamine;
palladium on activated charcoal;
In
methanol; water; ethyl acetate;
1: Ring cleavage / 2: Catalytic hydrogenation;
DOI:10.1016/S0223-5234(00)00114-8
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 62 percent / pyridine / 48 h / 20 °C
2: H2; NEt3 / 10 percent Pd-C / ethyl acetate / 18 h / 760 Torr
3: 85 percent / NaOMe / methanol; CHCl3 / 20 °C
4: 55 percent / NaN3; NH4Cl / methanol; H2O / 24 h / Heating
5: 81 percent / H2; Et3N / 10 percent Pd-C / ethyl acetate / 760 Torr
With
pyridine; sodium azide; hydrogen; sodium methylate; ammonium chloride; triethylamine;
palladium on activated charcoal;
In
methanol; chloroform; water; ethyl acetate;
1: Tosylation / 2: Catalytic hydrogenation / 3: Epoxidation / 4: Ring cleavage / 5: Catalytic hydrogenation;
DOI:10.1016/S0223-5234(00)00114-8
