benzyl (1S)-1-[(1-tert-butyldimethylsilyl)oxymethyl]-4-oxotetradecylcarbamate

Base Information

Chemical Name:benzyl (1S)-1-[(1-tert-butyldimethylsilyl)oxymethyl]-4-oxotetradecylcarbamate
CAS No.:642410-61-5
Molecular Formula:C₂₉H₅₁NO₄Si
Molecular Weight:505.814
Hs Code.:

Synonyms:benzyl (1S)-1-[(1-tert-butyldimethylsilyl)oxymethyl]-4-oxotetradecylcarbamate

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Chemical Property of benzyl (1S)-1-[(1-tert-butyldimethylsilyl)oxymethyl]-4-oxotetradecylcarbamate

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Technology Process of benzyl (1S)-1-[(1-tert-butyldimethylsilyl)oxymethyl]-4-oxotetradecylcarbamate

There total 3 articles about benzyl (1S)-1-[(1-tert-butyldimethylsilyl)oxymethyl]-4-oxotetradecylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 642410-54-6
benzyl (1S)-1-[(1-tert-butyldimethylsilyl)oxymethyl]-4-oxo-5-(phenylsulfonyl)tetradecylcarbamate

: 642410-61-5
benzyl (1S)-1-[(1-tert-butyldimethylsilyl)oxymethyl]-4-oxotetradecylcarbamate

Guidance literature:: With sodium amalgam; camphor-10-sulfonic acid; In methanol; at 20 ℃;
DOI:10.1002/ejoc.200300393

Reference yield:

: 96550-93-5
(decane-1-sulfonyl)benzene

: 642410-61-5
benzyl (1S)-1-[(1-tert-butyldimethylsilyl)oxymethyl]-4-oxotetradecylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / nBuLi / tetrahydrofuran; hexane / -72 °C

2: 92 percent / sodium amalgam; NaHPO₄ / methanol / 20 °C

With sodium amalgam; n-butyllithium; camphor-10-sulfonic acid; In tetrahydrofuran; methanol; hexane;
DOI:10.1002/ejoc.200300393

Reference yield:

: 153870-09-8
(S)-1-(benzyloxycarbonyl)-5-[(tert-butyldimethylsilyl)oxymethyl]-2-pyrrolidinone

: 642410-61-5
benzyl (1S)-1-[(1-tert-butyldimethylsilyl)oxymethyl]-4-oxotetradecylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / nBuLi / tetrahydrofuran; hexane / -72 °C

2: 92 percent / sodium amalgam; NaHPO₄ / methanol / 20 °C

With sodium amalgam; n-butyllithium; camphor-10-sulfonic acid; In tetrahydrofuran; methanol; hexane;
DOI:10.1002/ejoc.200300393