N-benzyloxycarbonyl-L-isoleucyl-1-amino-N,N-dimethylcyclobutancarboxamid

Base Information

Chemical Name:N-benzyloxycarbonyl-L-isoleucyl-1-amino-N,N-dimethylcyclobutancarboxamid
CAS No.:112142-73-1
Molecular Formula:C₂₁H₃₁N₃O₄
Molecular Weight:389.495
Hs Code.:

Synonyms:N-benzyloxycarbonyl-L-isoleucyl-1-amino-N,N-dimethylcyclobutancarboxamid

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Chemical Property of N-benzyloxycarbonyl-L-isoleucyl-1-amino-N,N-dimethylcyclobutancarboxamid

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Technology Process of N-benzyloxycarbonyl-L-isoleucyl-1-amino-N,N-dimethylcyclobutancarboxamid

There total 1 articles about N-benzyloxycarbonyl-L-isoleucyl-1-amino-N,N-dimethylcyclobutancarboxamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 3160-59-6
N-Cbz-L-Isoleucine

: 112142-86-6
2-dimethylamino-1-azaspiro<2.3>hex-1-ene

: 112142-73-1
N-benzyloxycarbonyl-L-isoleucyl-1-amino-N,N-dimethylcyclobutancarboxamid

Guidance literature:: In diethyl ether; at 0 ℃; for 0.0833333h;
DOI:10.1002/hlca.19870700213

Reference yield: 90.0%

: 112142-73-1
N-benzyloxycarbonyl-L-isoleucyl-1-amino-N,N-dimethylcyclobutancarboxamid

: 112142-83-3
N-(benzyloxycarbonyl)-L-isoleucyl-1-aminocyclobutancarbonsaure

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; at 35 ℃; for 100h;
DOI:10.1002/hlca.19870700213

Reference yield:

: 112142-73-1
N-benzyloxycarbonyl-L-isoleucyl-1-amino-N,N-dimethylcyclobutancarboxamid

: N-(benzyloxycarbonyl)-L-isoleucyl-1-aminocyclobutancarbonyl-4-aminobenzoesaure-ethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 3N HCl / tetrahydrofuran; H₂O / 100 h / 35 °C

2: 1.) DCC, 2.) CSA / 1.) CH₂Cl₂, 0 deg C, 5 min, 2.) CH₂Cl₂, room temperature

With hydrogenchloride; camphor-10-sulfonic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran; water;
DOI:10.1002/hlca.19880710118