bis-pentafluorophenyl 2-isopropyl-cycloprop-2-ene-1,1-bis-carboxylic ester

Base Information

Chemical Name:bis-pentafluorophenyl 2-isopropyl-cycloprop-2-ene-1,1-bis-carboxylic ester
CAS No.:905845-22-9
Molecular Formula:C₂₀H₈F₁₀O₄
Molecular Weight:502.265
Hs Code.:

Synonyms:bis-pentafluorophenyl 2-isopropyl-cycloprop-2-ene-1,1-bis-carboxylic ester

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Chemical Property of bis-pentafluorophenyl 2-isopropyl-cycloprop-2-ene-1,1-bis-carboxylic ester

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Technology Process of bis-pentafluorophenyl 2-isopropyl-cycloprop-2-ene-1,1-bis-carboxylic ester

There total 3 articles about bis-pentafluorophenyl 2-isopropyl-cycloprop-2-ene-1,1-bis-carboxylic ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 905845-06-9
2-isopropyl-cycloprop-2-ene-1,1-dicarboxylic acid

: 14533-84-7
pentafluorophenyl trifloroacetate

: 905845-22-9
bis-pentafluorophenyl 2-isopropyl-cycloprop-2-ene-1,1-bis-carboxylic ester

Guidance literature:: With triethylamine; In tetrahydrofuran; for 0.5h; cooling;
DOI:10.1021/ol060847l

Reference yield:

: 598-23-2
3-methyl-but-1-yne

: 905845-22-9
bis-pentafluorophenyl 2-isopropyl-cycloprop-2-ene-1,1-bis-carboxylic ester

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / Rh₂(OAc)4 / CH₂Cl₂ / 20 °C

2: 99 percent / NaOH / methanol; H₂O / 14 h / 20 °C

3: 78 percent / triethylamine / tetrahydrofuran / 0.5 h / cooling

With sodium hydroxide; triethylamine; dirhodium tetraacetate; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/ol060847l

Reference yield:

: 905844-91-9
dimethyl 2-isopropyl-cycloprop-2-ene-1,1-dicarboxylic ester

: 905845-22-9
bis-pentafluorophenyl 2-isopropyl-cycloprop-2-ene-1,1-bis-carboxylic ester

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / NaOH / methanol; H₂O / 14 h / 20 °C

2: 78 percent / triethylamine / tetrahydrofuran / 0.5 h / cooling

With sodium hydroxide; triethylamine; In tetrahydrofuran; methanol; water;
DOI:10.1021/ol060847l