2-(trimethylsilyl)ethyl 2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

Base Information

Chemical Name:2-(trimethylsilyl)ethyl 2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside
CAS No.:678995-59-0
Molecular Formula:C₂₅H₃₄O₆Si
Molecular Weight:458.627
Hs Code.:

Synonyms:2-(trimethylsilyl)ethyl 2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

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Chemical Property of 2-(trimethylsilyl)ethyl 2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

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Technology Process of 2-(trimethylsilyl)ethyl 2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

There total 8 articles about 2-(trimethylsilyl)ethyl 2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 678995-75-0
2-(trimethylsilyl)ethyl 2-O-benzyl-4,6-O-benzylidene-3-O-(4-methoxybenzyl)-β-D-galactopyranoside

: 678995-59-0
2-(trimethylsilyl)ethyl 2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

Guidance literature:: With ammonium cerium(IV) nitrate; In acetonitrile; at 20 ℃; for 1h;
DOI:10.1021/ol036460p

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 678995-59-0
2-(trimethylsilyl)ethyl 2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: p-toluenesulfonic acid / acetonitrile / 0.42 h / 20 °C

2: 0.877 g / NaH / dimethylformamide / 3 h / 20 °C

3: 77 percent / aq. ceric ammomium nitrate / acetonitrile / 1 h / 20 °C

With ammonium cerium(IV) nitrate; sodium hydride; toluene-4-sulfonic acid; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol036460p

Reference yield:

: 143834-54-2
2-(trimethylsilyl)ethyl 3-O-p-methoxybenzyl-β-D-galactopyranoside

: 678995-59-0
2-(trimethylsilyl)ethyl 2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: p-toluenesulfonic acid / acetonitrile / 0.42 h / 20 °C

2: 0.877 g / NaH / dimethylformamide / 3 h / 20 °C

3: 77 percent / aq. ceric ammomium nitrate / acetonitrile / 1 h / 20 °C

With ammonium cerium(IV) nitrate; sodium hydride; toluene-4-sulfonic acid; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol036460p