di-boc-1-(2-(5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)ethyl)hydrazine

Base Information

Chemical Name:di-boc-1-(2-(5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)ethyl)hydrazine
CAS No.:1018783-75-9
Molecular Formula:C₂₆H₃₂F₂N₄O₄S
Molecular Weight:534.627
Hs Code.:

Synonyms:di-boc-1-(2-(5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)ethyl)hydrazine

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Chemical Property of di-boc-1-(2-(5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)ethyl)hydrazine

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Technology Process of di-boc-1-(2-(5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)ethyl)hydrazine

There total 2 articles about di-boc-1-(2-(5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)ethyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 885060-36-6
2,5-difluoro-benzothiohydrazide

: 1018783-73-7
N,N'-di-boc-3-hydrazinyl-1-phenylpropan-1-one

: 1018783-75-9
di-boc-1-(2-(5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)ethyl)hydrazine

Guidance literature:: In ethanol; at 20 ℃; for 72h;

Reference yield:

: 1021853-64-4
C₇H₄F₂S₂

: 1018783-75-9
di-boc-1-(2-(5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)ethyl)hydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / water / 14 h / 20 °C

2: sodium hydroxide; hydrazine / 14 h / 0 - 20 °C

3: ethanol / 72 h / 20 °C

With sodium hydroxide; sodium hydrogencarbonate; hydrazine; In ethanol; water;

Reference yield: 54.0%

: 23953-00-6
(S)-2-methoxypropanoic acid

: 1018783-75-9
di-boc-1-(2-(5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)ethyl)hydrazine

: 1018783-78-2
C₃₀H₃₈F₂N₄O₆S

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 4.08333h;