2-iodo-4-phenoxybenzoic acid

Base Information

Chemical Name:2-iodo-4-phenoxybenzoic acid
CAS No.:910240-93-6
Molecular Formula:C₁₃H₉IO₃
Molecular Weight:340.117
Hs Code.:

Synonyms:2-iodo-4-phenoxybenzoic acid

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Chemical Property of 2-iodo-4-phenoxybenzoic acid

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Technology Process of 2-iodo-4-phenoxybenzoic acid

There total 5 articles about 2-iodo-4-phenoxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 910240-91-4
2-amino-4-phenoxybenzoic acid

: 910240-93-6
2-iodo-4-phenoxybenzoic acid

Guidance literature:: 2-amino-4-phenoxybenzoic acid; With sulfuric acid; acetic acid; sodium nitrite; In water; at 4 ℃; for 0.5h;

With potassium iodide; In water; at 4 - 20 ℃; for 3h;

Reference yield:

: 467462-17-5
1-methyl-2-nitro-4-phenoxybenzene

: 910240-93-6
2-iodo-4-phenoxybenzoic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: iron; acetic acid / methanol / 5 h / Heating / reflux

1.2: 20 °C

1.3: 0 °C

2.1: pyridine / dichloromethane / 6.5 h / 0 - 20 °C

3.1: potassium permanganate; magnesium sulfate / water; tert-butyl alcohol / 4 h / 20 °C / Heating / reflux

4.1: hydrazine / 4 h / Heating / reflux

5.1: sulfuric acid; acetic acid; sodium nitrite / water / 0.5 h / 4 °C

5.2: 3 h / 4 - 20 °C

With pyridine; potassium permanganate; sulfuric acid; iron; magnesium sulfate; acetic acid; hydrazine; sodium nitrite; In methanol; dichloromethane; water; tert-butyl alcohol;

Reference yield:

: 890315-89-6
2-methyl-5-phenoxyaniline hydrochloride

: 910240-93-6
2-iodo-4-phenoxybenzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine / dichloromethane / 6.5 h / 0 - 20 °C

2.1: potassium permanganate; magnesium sulfate / water; tert-butyl alcohol / 4 h / 20 °C / Heating / reflux

3.1: hydrazine / 4 h / Heating / reflux

4.1: sulfuric acid; acetic acid; sodium nitrite / water / 0.5 h / 4 °C

4.2: 3 h / 4 - 20 °C

With pyridine; potassium permanganate; sulfuric acid; magnesium sulfate; acetic acid; hydrazine; sodium nitrite; In dichloromethane; water; tert-butyl alcohol;