C₄₁H₆₀O₉Si

Base Information

Chemical Name:C₄₁H₆₀O₉Si
CAS No.:1264756-73-1
Molecular Formula:C₄₁H₆₀O₉Si
Molecular Weight:725.007
Hs Code.:

C<sub>41</sub>H<sub>60</sub>O<sub>9</sub>Si

Synonyms:C₄₁H₆₀O₉Si

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Chemical Property of C₄₁H₆₀O₉Si

Chemical Property:

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Technology Process of C₄₁H₆₀O₉Si

There total 42 articles about C₄₁H₆₀O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1264756-82-2
C₄₁H₆₀O₁₀Si

: 1264756-73-1
C₄₁H₆₀O₉Si

Guidance literature:: With triethylsilane; trimethylsilyl trifluoromethanesulfonate; In propiononitrile; at -78 ℃;
DOI:10.1016/j.tetlet.2010.11.127

Reference yield: 72.0%

: 1264756-72-0
C₅₃H₈₈O₁₀Si₃

: 1264756-73-1
C₄₁H₆₀O₉Si

Guidance literature:: With triethylsilane; trimethylsilyl trifluoromethanesulfonate; In propiononitrile; at -78 ℃;
DOI:10.1016/j.tetlet.2010.11.127

Reference yield:

: C₄₄H₅₂O₅Si

: 1264756-73-1
C₄₁H₆₀O₉Si

Guidance literature:: Multi-step reaction with 23 steps

1.1: water; potassium hydroxide / tetrahydrofuran; methanol

2.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 20 °C

2.2: 20 °C

3.1: diisobutylaluminium hydride / dichloromethane / -78 °C

4.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -40 °C / Molecular sieve

5.1: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide / dichloromethane; water / 0 °C

6.1: sodium hexamethyldisilazane / tetrahydrofuran / 0 °C

7.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 20 °C

8.1: potassium tert-butylate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 20 °C

9.1: bis-(1,2-dimethylpropyl)borane / tetrahydrofuran / 0 - 20 °C

9.2: 20 °C

10.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 20 °C

11.1: diethyl ether / -78 °C

12.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 20 °C / Molecular sieve

13.1: di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine / diethyl ether / 0 °C

13.2: -78 °C

14.1: Dess-Martin periodane / dichloromethane; tert-butyl alcohol / 20 °C

15.1: pyridinium p-toluenesulfonate / methanol / 80 °C

16.1: 2,6-dimethylpyridine / N,N-dimethyl-formamide / 20 °C

17.1: sodium tetrahydroborate; cerium(III) chloride / methanol; dichloromethane / 0 °C

18.1: boron trifluoride tetrahydrofuran complex / tetrahydrofuran / 0 °C

18.2: 0 - 20 °C

19.1: 2,6-dimethylpyridine / dichloromethane / 20 °C

20.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0 °C

21.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0 - 20 °C / Molecular sieve

22.1: toluene-4-sulfonic acid / methanol; dichloromethane / 20 °C

23.1: triethylsilane; trimethylsilyl trifluoromethanesulfonate / propiononitrile / -78 °C

With 2,6-dimethylpyridine; titanium(IV) isopropylate; triethylsilane; tert.-butylhydroperoxide; sodium hypochlorite; sodium tetrahydroborate; cerium(III) chloride; tetrapropylammonium perruthennate; oxalyl dichloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; boron trifluoride tetrahydrofuran complex; diethyl (2R,3R)-tartrate; trimethylsilyl trifluoromethanesulfonate; di-n-butylboryl trifluoromethanesulfonate; potassium tert-butylate; water; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; bis-(1,2-dimethylpropyl)borane; tetra-(n-butyl)ammonium iodide; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; toluene-4-sulfonic acid; dimethyl sulfoxide; 4-methylmorpholine N-oxide; triethylamine; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium bromide; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; propiononitrile; tert-butyl alcohol; 2.1: Swern oxidation / 2.2: Wittig reaction / 4.1: Sharpless asymmetric epoxidation / 6.1: Wittig reaction / 11.1: Grignard reaction / 14.1: Dess-Martin oxidation / 17.1: Luche reduction;
DOI:10.1016/j.tetlet.2010.11.127