[η4-1,3-bis(trimethylsilyl)-2-(1-phenylethyl)cyclobutadiene](η5-cyclopentadienyl)cobalt

Base Information

Chemical Name:[η4-1,3-bis(trimethylsilyl)-2-(1-phenylethyl)cyclobutadiene](η5-cyclopentadienyl)cobalt
CAS No.:90458-30-3
Molecular Formula:C₂₃H₃₃CoSi₂
Molecular Weight:424.679
Hs Code.:

Synonyms:[η4-1,3-bis(trimethylsilyl)-2-(1-phenylethyl)cyclobutadiene](η5-cyclopentadienyl)cobalt

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [η4-1,3-bis(trimethylsilyl)-2-(1-phenylethyl)cyclobutadiene](η5-cyclopentadienyl)cobalt

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Technology Process of [η4-1,3-bis(trimethylsilyl)-2-(1-phenylethyl)cyclobutadiene](η5-cyclopentadienyl)cobalt

There total 3 articles about [η4-1,3-bis(trimethylsilyl)-2-(1-phenylethyl)cyclobutadiene](η5-cyclopentadienyl)cobalt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 78341-15-8
[η4-1,2,3-tris(trimethylsilyl)-4-(1-phenylethyl)cyclobutadiene](η5-cyclopentadienyl)cobalt

: 90458-30-3
[η4-1,3-bis(trimethylsilyl)-2-(1-phenylethyl)cyclobutadiene](η5-cyclopentadienyl)cobalt

Guidance literature:: With toluene-4-sulfonic acid; In benzene-d6;
DOI:10.1021/ja00407a067

Reference yield: 75.0%

: 78341-15-8
[η4-1,2,3-tris(trimethylsilyl)-4-(1-phenylethyl)cyclobutadiene](η5-cyclopentadienyl)cobalt

: 6192-52-5
p-toluenesulfonic acid monohydrate

: 90458-30-3
[η4-1,3-bis(trimethylsilyl)-2-(1-phenylethyl)cyclobutadiene](η5-cyclopentadienyl)cobalt

Guidance literature:: In benzene-d6; Sonication; The soln. of reagents in C6D6 in NMR tube was subjected to sonic vibration for 2 h at 30°C;; HPLC with methanol, recrystd. from pentane;;
DOI:10.1021/om00086a007