C₁₄H₂₁O₁₃P₃

Base Information

Chemical Name:C₁₄H₂₁O₁₃P₃
CAS No.:1428631-97-3
Molecular Formula:C₁₄H₂₁O₁₃P₃
Molecular Weight:490.234
Hs Code.:

C<sub>14</sub>H<sub>21</sub>O<sub>13</sub>P<sub>3</sub>

Synonyms:C₁₄H₂₁O₁₃P₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₂₁O₁₃P₃

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Technology Process of C₁₄H₂₁O₁₃P₃

There total 6 articles about C₁₄H₂₁O₁₃P₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 1428631-93-9
C₁₄H₁₈O₄

: 1428631-97-3
C₁₄H₂₁O₁₃P₃

Guidance literature:: C₁₄H₁₈O₄; With trimethyl phosphite; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trichlorophosphate; at -15 - 10 ℃; Inert atmosphere;

With tributyl-amine; bis(tri-n-butylammonium) pyrophosphate; In N,N-dimethyl-formamide; at -10 - 0 ℃; for 0.5h;
DOI:10.1021/ja312148q

Reference yield:

: 1364927-25-2
C₂₀H₂₃NO₆

: 1428631-97-3
C₁₄H₂₁O₁₃P₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridine / 15 h / 20 °C / Inert atmosphere

2.1: triethylamine; palladium 10% on activated carbon; hydrogen / ethyl acetate / 1 h / 20 °C

3.1: hydrogenchloride / tetrahydrofuran; water / 0.25 h / 0 °C

3.2: 0.67 h / 0 °C

3.3: 2.6 h / 0 - 20 °C

4.1: copper(l) iodide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenyl-arsane / 1,4-dioxane / 2 h / 50 - 55 °C

5.1: sodium methylate / dichloromethane; methanol / 0.75 h / 5 - 20 °C

6.1: trimethyl phosphite; trichlorophosphate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / -15 - 10 °C / Inert atmosphere

6.2: 0.5 h / -10 - 0 °C

With pyridine; trimethyl phosphite; hydrogenchloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; triphenyl-arsane; palladium 10% on activated carbon; hydrogen; sodium methylate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; triethylamine; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; ethyl acetate; 3.2: |Sandmeyer Reaction / 3.3: |Sandmeyer Reaction / 4.1: |Stille Cross Coupling;
DOI:10.1021/ja312148q

Reference yield:

: 1428631-84-8
C₂₈H₂₉NO₆

: 1428631-97-3
C₁₄H₂₁O₁₃P₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride / tetrahydrofuran; water / 0.25 h / 0 °C

1.2: 0.67 h / 0 °C

1.3: 2.6 h / 0 - 20 °C

2.1: copper(l) iodide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenyl-arsane / 1,4-dioxane / 2 h / 50 - 55 °C

3.1: sodium methylate / dichloromethane; methanol / 0.75 h / 5 - 20 °C

4.1: trimethyl phosphite; trichlorophosphate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / -15 - 10 °C / Inert atmosphere

4.2: 0.5 h / -10 - 0 °C

With trimethyl phosphite; hydrogenchloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; triphenyl-arsane; sodium methylate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; 1.2: |Sandmeyer Reaction / 1.3: |Sandmeyer Reaction / 2.1: |Stille Cross Coupling;
DOI:10.1021/ja312148q