Technology Process of 3,8-diamino-5-ethyl-6-phenylphenanthridinium ethyl sulfate
There total 8 articles about 3,8-diamino-5-ethyl-6-phenylphenanthridinium ethyl sulfate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
3,8-dicarboethoxyamino-5-ethyl-6-phenylphenanthridinium ethyl sulfate;
With
sulfuric acid;
In
water;
at 140 ℃;
for 1h;
With
ammonia;
In
water;
DOI:10.1134/S107042721109014X
- Guidance literature:
-
Multi-step reaction with 7 steps
1: hydrogen / ethanol / 60 °C / 22052.2 Torr
2: sulfuric acid; potassium nitrate
3: tin(IV) chloride / nitrobenzene
4: hydrazine hydrate / ethanol / 1 h / 75 °C
5: pyridine
6: nitrobenzene / 0.5 h / 165 °C
7: sulfuric acid / water / 1 h / 140 °C
With
pyridine; hydrazine hydrate; sulfuric acid; hydrogen; tin(IV) chloride; potassium nitrate;
In
ethanol; water; nitrobenzene;
DOI:10.1134/S107042721109014X
- Guidance literature:
-
Multi-step reaction with 2 steps
1: nitrobenzene / 0.5 h / 165 °C
2: sulfuric acid / water / 1 h / 140 °C
With
sulfuric acid;
In
water; nitrobenzene;
DOI:10.1134/S107042721109014X
