methyl 3,6-diazido-4-O-benzoyl-2,3,6-trideoxy-α-D-arabino-hexopyranoside

Base Information

Chemical Name:methyl 3,6-diazido-4-O-benzoyl-2,3,6-trideoxy-α-D-arabino-hexopyranoside
CAS No.:98383-24-5
Molecular Formula:C₁₄H₁₆N₆O₄
Molecular Weight:332.319
Hs Code.:

Synonyms:methyl 3,6-diazido-4-O-benzoyl-2,3,6-trideoxy-α-D-arabino-hexopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3,6-diazido-4-O-benzoyl-2,3,6-trideoxy-α-D-arabino-hexopyranoside

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Technology Process of methyl 3,6-diazido-4-O-benzoyl-2,3,6-trideoxy-α-D-arabino-hexopyranoside

There total 1 articles about methyl 3,6-diazido-4-O-benzoyl-2,3,6-trideoxy-α-D-arabino-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 18933-62-5
methyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-α-D-arabino-hexopyranoside

: 98383-24-5
methyl 3,6-diazido-4-O-benzoyl-2,3,6-trideoxy-α-D-arabino-hexopyranoside

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 80 ℃; for 8h;
DOI:10.1021/jm00121a005

Reference yield:

: 98383-24-5
methyl 3,6-diazido-4-O-benzoyl-2,3,6-trideoxy-α-D-arabino-hexopyranoside

: 98383-27-8
C₁₃H₂₂Cl₂N₆O₇

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / 2 N aq. NaOH / methanol / 2 h

2: 100 percent / H₂, Et₃N / 10percent Pd/C / ethanol

3: dimethylformamide / 5 h / 0 °C

4: sodium nitrite / formic acid / 0.5 h

With sodium hydroxide; hydrogen; triethylamine; sodium nitrite; palladium on activated charcoal; In methanol; formic acid; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00121a005