3,3-Diethoxy-1-[4-(4-methoxy-phenyl)-1-methyl-cyclohex-3-enyl]-propan-1-one

Base Information

Chemical Name:3,3-Diethoxy-1-[4-(4-methoxy-phenyl)-1-methyl-cyclohex-3-enyl]-propan-1-one
CAS No.:99034-38-5
Molecular Formula:C₂₁H₃₀O₄
Molecular Weight:346.467
Hs Code.:

Synonyms:3,3-Diethoxy-1-[4-(4-methoxy-phenyl)-1-methyl-cyclohex-3-enyl]-propan-1-one

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Chemical Property of 3,3-Diethoxy-1-[4-(4-methoxy-phenyl)-1-methyl-cyclohex-3-enyl]-propan-1-one

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Technology Process of 3,3-Diethoxy-1-[4-(4-methoxy-phenyl)-1-methyl-cyclohex-3-enyl]-propan-1-one

There total 1 articles about 3,3-Diethoxy-1-[4-(4-methoxy-phenyl)-1-methyl-cyclohex-3-enyl]-propan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122-51-0
orthoformic acid triethyl ester

: 99034-26-1
1-[4-(4-Methoxy-phenyl)-1-methyl-cyclohex-3-enyl]-ethanone

: 99034-38-5
3,3-Diethoxy-1-[4-(4-methoxy-phenyl)-1-methyl-cyclohex-3-enyl]-propan-1-one

Guidance literature:: With boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; Yield given. Multistep reaction; 1.) CH₂Cl₂, 0 deg C, 15 min, 2.) CH₂Cl₂, -20 deg C to -10 deg C, 2 h;
DOI:10.1021/jo00225a054

Reference yield:

: 99034-38-5
3,3-Diethoxy-1-[4-(4-methoxy-phenyl)-1-methyl-cyclohex-3-enyl]-propan-1-one

: 99034-51-2
6-(4-Methoxy-phenyl)-1-methyl-bicyclo[3.3.1]nona-3,6-dien-2-one

Guidance literature:: With perchloric acid; In benzene; at 0 - 20 ℃; for 3h; Yield given;
DOI:10.1021/jo00225a054

Reference yield:

: 99034-38-5
3,3-Diethoxy-1-[4-(4-methoxy-phenyl)-1-methyl-cyclohex-3-enyl]-propan-1-one

: 99034-59-0
6-(4-Methoxy-phenyl)-1-methyl-bicyclo[3.3.1]non-6-en-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 70percent aq. HClO₄ / benzene / 3 h / 0 - 20 °C

2: H₂ / 10percent Pd/C / various solvent(s) / 2 h / 760 Torr / Ambient temperature

With perchloric acid; hydrogen; palladium on activated charcoal; In benzene;
DOI:10.1021/jo00225a054