FA-PHE-OME

Base Information

• Chemical Name: FA-PHE-OME
• CAS No.: 36020-63-0
• Molecular Formula: C17H17 N O4
• Molecular Weight: 299.32
• Hs Code.: 2932190090
• Mol file: 36020-63-0.mol

Synonyms:L-Phenylalanine,N-[(2E)-3-(2-furanyl)-1-oxo-2-propenyl]-, methyl ester (9CI); L-Phenylalanine,N-[3-(2-furanyl)-1-oxo-2-propenyl]-, methyl ester, (E)-;N-trans-(2-Furyl)acryloyl-L-phenylalanine methyl ester

Chemical Property of FA-PHE-OME

Chemical Property:

• PSA: 68.54000
• LogP: 2.58420
• Storage Temp.: -15°C

Purity/Quality:

99% ^*data from raw suppliers

(S,E)-Methyl2-(3-(furan-2-yl)acrylamido)-3-phenylpropanoate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of FA-PHE-OME

There total 2 articles about FA-PHE-OME which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

methyl (2S)-2-amino-3-phenylpropanoate hydrochloride (7524-50-7) + 3-(fur-2-yl)crotonic acid (539-47-9,15690-24-1) → N-trans-(2-Furyl)acryloyl-L-phenylalanin-methylester (36020-63-0)

Guidance literature:

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 12h;

DOI:10.1016/j.tetlet.2004.11.082

Reference yield:

→ N-trans-(2-Furyl)acryloyl-L-phenylalanin-methylester (36020-63-0)

Guidance literature:

aus L-Phenylalaninmethylester, Furacryloylchlorid;

Reference yield: 88.0%

N-trans-(2-Furyl)acryloyl-L-phenylalanin-methylester (36020-63-0) → fa-Phe

Guidance literature:

With sodium hydroxide; In 1,4-dioxane; at 20 ℃; for 12h;

DOI:10.1016/j.tetlet.2004.11.082

upstream raw materials:

methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

3-(fur-2-yl)crotonic acid

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