N-{2-[(anthracen-9-ylmethyl)amino]ethyl}-N'-(2-{2-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]ethylamino}ethyl)ethane-1,2-diamine

Base Information

Chemical Name:N-{2-[(anthracen-9-ylmethyl)amino]ethyl}-N'-(2-{2-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]ethylamino}ethyl)ethane-1,2-diamine
CAS No.:1391748-74-5
Molecular Formula:C₄₁H₅₀N₆O₂
Molecular Weight:658.887
Hs Code.:

Synonyms:N-{2-[(anthracen-9-ylmethyl)amino]ethyl}-N'-(2-{2-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]ethylamino}ethyl)ethane-1,2-diamine

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Chemical Property of N-{2-[(anthracen-9-ylmethyl)amino]ethyl}-N'-(2-{2-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]ethylamino}ethyl)ethane-1,2-diamine

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Technology Process of N-{2-[(anthracen-9-ylmethyl)amino]ethyl}-N'-(2-{2-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]ethylamino}ethyl)ethane-1,2-diamine

There total 5 articles about N-{2-[(anthracen-9-ylmethyl)amino]ethyl}-N'-(2-{2-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]ethylamino}ethyl)ethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1391748-87-0
{2-[(anthracen-9-ylmethyl)amino]ethyl}-(2-{tert-butoxycarbonyl-[2-(tert-butoxycarbonyl-{2-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]ethyl}amino)ethyl]amino}ethyl)carbamic acid tert-butyl ester

: 1391748-74-5
N-{2-[(anthracen-9-ylmethyl)amino]ethyl}-N'-(2-{2-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]ethylamino}ethyl)ethane-1,2-diamine

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1002/anie.201200822

Reference yield:

: 642-31-9
9-anthracene aldehyde

: 1391748-74-5
N-{2-[(anthracen-9-ylmethyl)amino]ethyl}-N'-(2-{2-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]ethylamino}ethyl)ethane-1,2-diamine

Guidance literature:: Multi-step reaction with 4 steps

1: ethanol / 72 h / 20 °C / Inert atmosphere

2: sodium tetrahydroborate / ethanol / 24 h / 20 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine / methanol / 72 h / 20 °C / Inert atmosphere

4: trifluoroacetic acid / dichloromethane / 5 h / 20 °C

With sodium tetrahydroborate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In methanol; ethanol; dichloromethane;
DOI:10.1002/anie.201200822

Reference yield:

: 1391748-86-9
[2-({2-[(2-aminoethyl)-tert-butoxycarbonylamino]ethyl}-tert-butoxycarbonylamino)ethyl]-[2-(3-phenylpropylamino)ethyl]carbamic acid tert-butyl ester

: 1391748-74-5
N-{2-[(anthracen-9-ylmethyl)amino]ethyl}-N'-(2-{2-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]ethylamino}ethyl)ethane-1,2-diamine

Guidance literature:: Multi-step reaction with 4 steps

1: ethanol / 72 h / 20 °C / Inert atmosphere

2: sodium tetrahydroborate / ethanol / 24 h / 20 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine / methanol / 72 h / 20 °C / Inert atmosphere

4: trifluoroacetic acid / dichloromethane / 5 h / 20 °C

With sodium tetrahydroborate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In methanol; ethanol; dichloromethane;
DOI:10.1002/anie.201200822