5,6,7,8-tetrahydro-5,9,9-trimethyl-3-(3-nitrophenyl)-5,8-methano-1,2,4-benzotriazine

Base Information

Chemical Name:5,6,7,8-tetrahydro-5,9,9-trimethyl-3-(3-nitrophenyl)-5,8-methano-1,2,4-benzotriazine
CAS No.:84831-92-5
Molecular Formula:C₁₇H₁₈N₄O₂
Molecular Weight:310.356
Hs Code.:

Synonyms:5,6,7,8-tetrahydro-5,9,9-trimethyl-3-(3-nitrophenyl)-5,8-methano-1,2,4-benzotriazine

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Chemical Property of 5,6,7,8-tetrahydro-5,9,9-trimethyl-3-(3-nitrophenyl)-5,8-methano-1,2,4-benzotriazine

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Technology Process of 5,6,7,8-tetrahydro-5,9,9-trimethyl-3-(3-nitrophenyl)-5,8-methano-1,2,4-benzotriazine

There total 2 articles about 5,6,7,8-tetrahydro-5,9,9-trimethyl-3-(3-nitrophenyl)-5,8-methano-1,2,4-benzotriazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.0%

: 2767-84-2,10334-26-6,10373-78-1,71074-96-9,105309-30-6,465-29-2
Camphorquinone

: 60666-23-1
3-nitrobenzenecarboximidohydrazide

: 84831-92-5
5,6,7,8-tetrahydro-5,9,9-trimethyl-3-(3-nitrophenyl)-5,8-methano-1,2,4-benzotriazine

: 84831-93-6
5,6,7,8-tetrahydro-8,9,9-trimethyl-3-(3-nitrophenyl)-5,8-methano-1,2,4-benzotriazine

Guidance literature:: In isopropyl alcohol; for 8h; Heating;

Reference yield:

: 831-65-2
ethyl 3-nitrobenzenecarboximidate

: 84831-92-5
5,6,7,8-tetrahydro-5,9,9-trimethyl-3-(3-nitrophenyl)-5,8-methano-1,2,4-benzotriazine

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / hydrazine hydrate / propan-2-ol / 7 h / 45 °C

2: 14.7 percent / propan-2-ol / 8 h / Heating

With hydrazine hydrate; In isopropyl alcohol;