benzyl 2-deoxy-2-<(3R)-3-dodecanoyloxytetradecanamido>-4,6-O-isopropylidene-β-D-glucopyranoside

Base Information

Chemical Name:benzyl 2-deoxy-2-<(3R)-3-dodecanoyloxytetradecanamido>-4,6-O-isopropylidene-β-D-glucopyranoside
CAS No.:106022-61-1
Molecular Formula:C₄₂H₇₁NO₈
Molecular Weight:718.028
Hs Code.:

Synonyms:benzyl 2-deoxy-2-<(3R)-3-dodecanoyloxytetradecanamido>-4,6-O-isopropylidene-β-D-glucopyranoside

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Chemical Property of benzyl 2-deoxy-2-<(3R)-3-dodecanoyloxytetradecanamido>-4,6-O-isopropylidene-β-D-glucopyranoside

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Technology Process of benzyl 2-deoxy-2-<(3R)-3-dodecanoyloxytetradecanamido>-4,6-O-isopropylidene-β-D-glucopyranoside

There total 5 articles about benzyl 2-deoxy-2-<(3R)-3-dodecanoyloxytetradecanamido>-4,6-O-isopropylidene-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 107856-74-6
C₂₆H₅₀O₄

: 102794-17-2
benzyl 2-amino-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

: 106022-61-1
benzyl 2-deoxy-2-<(3R)-3-dodecanoyloxytetradecanamido>-4,6-O-isopropylidene-β-D-glucopyranoside

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; Ambient temperature;
DOI:10.1016/0008-6215(87)80220-3

Reference yield: 51.0%

: 107856-74-6
C₂₆H₅₀O₄

: 102794-17-2
benzyl 2-amino-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

: 115288-02-3
Dodecanoic acid ((4aR,6R,7R,8R,8aS)-6-benzyloxy-8-hydroxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-amide

: 106022-61-1
benzyl 2-deoxy-2-<(3R)-3-dodecanoyloxytetradecanamido>-4,6-O-isopropylidene-β-D-glucopyranoside

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; for 4h; Mechanism; Ambient temperature;
DOI:10.1248/cpb.35.4517

Reference yield:

: 112-16-3
n-dodecanoyl chloride

: 106022-61-1
benzyl 2-deoxy-2-<(3R)-3-dodecanoyloxytetradecanamido>-4,6-O-isopropylidene-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 95.3 percent / DMAP / CH₂Cl₂; pyridine / Ambient temperature

2: zinc dust, acetic acid / 50 °C

3: 90 percent / 3-(3-dimethylamino)propyl-1-ethylcarbodiimide hydrochloride / CH₂Cl₂ / Ambient temperature

With dmap; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; zinc; In pyridine; dichloromethane;
DOI:10.1016/0008-6215(87)80220-3