(C₅H₅)Fe(C₅H₄C(C₆H₅)N(CH₂)5)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Fe(C₅H₄C(C₆H₅)N(CH₂)5)PF₆

Base Information

Chemical Name:(C₅H₅)Fe(C₅H₄C(C₆H₅)N(CH₂)5)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Fe(C₅H₄C(C₆H₅)N(CH₂)5)PF₆
CAS No.:75192-58-4
Molecular Formula:C₂₂H₂₄FeN*F₆P
Molecular Weight:503.25
Hs Code.:

(C<sub>5</sub>H<sub>5</sub>)Fe(C<sub>5</sub>H<sub>4</sub>C(C<sub>6</sub>H<sub>5</sub>)N(CH<sub>2</sub>)5)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=(C<sub>5</sub>H<sub>5</sub>)Fe(C<sub>5</sub>H<sub>4</sub>C(C<sub>6</sub>H<sub>5</sub>)N(CH<sub>2</sub>)5)PF<sub>6</sub>

Synonyms:(C₅H₅)Fe(C₅H₄C(C₆H₅)N(CH₂)5)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Fe(C₅H₄C(C₆H₅)N(CH₂)5)PF₆

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Chemical Property of (C₅H₅)Fe(C₅H₄C(C₆H₅)N(CH₂)5)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Fe(C₅H₄C(C₆H₅)N(CH₂)5)PF₆

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Technology Process of (C₅H₅)Fe(C₅H₄C(C₆H₅)N(CH₂)5)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Fe(C₅H₄C(C₆H₅)N(CH₂)5)PF₆

There total 1 articles about (C₅H₅)Fe(C₅H₄C(C₆H₅)N(CH₂)5)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Fe(C₅H₄C(C₆H₅)N(CH₂)5)PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 110-89-4
piperidine

: 1272-44-2
benzoylferrocene

: 75192-58-4
(C₅H₅)Fe(C₅H₄C(C₆H₅)N(CH₂)5)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Fe(C₅H₄C(C₆H₅)N(CH₂)5)PF₆

Guidance literature:: With aluminium chloride dimer; In 1,2-dichloro-ethane; slow addn. of amine to a stirred suspn. of finely powdered Al2Cl6 in dry ClCH2CH2Cl, stirring until complex formation is complete, addn. of aroylferrocene in ClCH2CH2Cl, stirring and heating to 90°C for 7 h under N2; pouring into water, sepn. of aq. layer, washing with ether, addn. of NH4PF6, extn. with CH2Cl2, drying extract (MgSO4), evapn. to low bulk under reduced pressure, pptn. by addn. of light petroleum, recrystn. from ether/CH2Cl2;

Reference yield:

: 75192-58-4
(C₅H₅)Fe(C₅H₄C(C₆H₅)N(CH₂)5)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Fe(C₅H₄C(C₆H₅)N(CH₂)5)PF₆

: 1272-44-2
benzoylferrocene

Guidance literature:: With sodium hydroxide; In water; acetonitrile; soln. of Fe complex in acetonitrile treated with aq. soln. of NaOH for 0.5 h; addn. of H2O, extn. (Et2O), washing with H2O, drying over MgSO4, evapn.;

Reference yield:

: 75192-58-4
(C₅H₅)Fe(C₅H₄C(C₆H₅)N(CH₂)5)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Fe(C₅H₄C(C₆H₅)N(CH₂)5)PF₆

: C₅H₅FeC₅H₄CH(C₆H₅)NC₅H₁₀

Guidance literature:: With sodium tetrahydroborate; In 1,2-dimethoxyethane; water; excess of NaBH4 added to soln. of Fe complex in 1,2-dimethoxyethane-water, mixture stirred for 1 h; addn. of H2O, extn. (Et2O), washing with H2O, drying over MgSO4, evapn.;