Carbamic acid, (1,2-dimethyl-2-propenyl)-, 1,1-dimethylethyl ester (9CI)

Base Information

Chemical Name:Carbamic acid, (1,2-dimethyl-2-propenyl)-, 1,1-dimethylethyl ester (9CI)
CAS No.:267668-39-3
Molecular Formula:C₁₀H₁₉NO₂
Molecular Weight:185.266
Hs Code.:
Mol file:267668-39-3.mol

Synonyms:Carbamic acid, (1,2-dimethyl-2-propenyl)-, 1,1-dimethylethyl ester (9CI)

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Chemical Property of Carbamic acid, (1,2-dimethyl-2-propenyl)-, 1,1-dimethylethyl ester (9CI)

Chemical Property:

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Technology Process of Carbamic acid, (1,2-dimethyl-2-propenyl)-, 1,1-dimethylethyl ester (9CI)

There total 3 articles about Carbamic acid, (1,2-dimethyl-2-propenyl)-, 1,1-dimethylethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 267668-29-1
N-tert-butyloxycarbonyl-N-(1,2-dimethyl-2-propenyl)benzenesulfenamide

: 267668-39-3
N-tert-butoxycarbonyl-N-(1,2-dimethyl-2-propenyl)amine

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 1h; Heating;
DOI:10.1021/jo991569p

Reference yield: 81.0%

: Ph₃PCH₃I

: (+/-)-tert-butyl (3-oxobutan-2-yl)carbamate

: 267668-39-3
N-tert-butoxycarbonyl-N-(1,2-dimethyl-2-propenyl)amine

Guidance literature:: Ph₃PCH₃I; With sodium hexamethyldisilazane; In tetrahydrofuran; toluene; at 0 ℃; for 0.25h; Inert atmosphere;

(+/-)-tert-butyl (3-oxobutan-2-yl)carbamate; In tetrahydrofuran; toluene; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol200323r

Reference yield:

: 1070-19-5
N-(tert-butyloxycarbonyl) azide

: 267668-39-3
N-tert-butoxycarbonyl-N-(1,2-dimethyl-2-propenyl)amine

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / FeCl₂ / CH₂Cl₂ / 20 °C

2: 90 percent / Bu₃SnH; AIBN / benzene / 1 h / Heating

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; iron(II) chloride; In dichloromethane; benzene; 1: Rearrangement / 2: desulfurization;
DOI:10.1021/jo991569p