tetramethyl-4,4,5,5 (dimethylaminomethyl-2 phenyl)-2 phenyl-2 dioxasilacyclopentane-1,3,2

Base Information

Chemical Name:tetramethyl-4,4,5,5 (dimethylaminomethyl-2 phenyl)-2 phenyl-2 dioxasilacyclopentane-1,3,2
CAS No.:133156-64-6
Molecular Formula:C₂₁H₂₉NO₂Si
Molecular Weight:355.552
Hs Code.:

Synonyms:tetramethyl-4,4,5,5 (dimethylaminomethyl-2 phenyl)-2 phenyl-2 dioxasilacyclopentane-1,3,2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetramethyl-4,4,5,5 (dimethylaminomethyl-2 phenyl)-2 phenyl-2 dioxasilacyclopentane-1,3,2

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Technology Process of tetramethyl-4,4,5,5 (dimethylaminomethyl-2 phenyl)-2 phenyl-2 dioxasilacyclopentane-1,3,2

There total 3 articles about tetramethyl-4,4,5,5 (dimethylaminomethyl-2 phenyl)-2 phenyl-2 dioxasilacyclopentane-1,3,2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 114499-75-1
(dimethylaminomethyl-2 phenyl)-1 phenylsilane

: 133156-64-6
tetramethyl-4,4,5,5 (dimethylaminomethyl-2 phenyl)-2 phenyl-2 dioxasilacyclopentane-1,3,2

Guidance literature:: In tetrachloromethane; at 77 ℃; for 15h;
DOI:10.1016/0022-328X(90)80080-J

Reference yield:

: 103-83-3
N,N'-dimethylbenzylamine

: 133156-64-6
tetramethyl-4,4,5,5 (dimethylaminomethyl-2 phenyl)-2 phenyl-2 dioxasilacyclopentane-1,3,2

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) Et₂O, hexane, rt, 48 h, 2.) rt, 48 h

2: 87 percent / CCl₄ / 15 h / 77 °C

With n-butyllithium; In tetrachloromethane;
DOI:10.1016/0022-328X(90)80080-J

Reference yield:

: 694-53-1
phenylsilane

: 133156-64-6
tetramethyl-4,4,5,5 (dimethylaminomethyl-2 phenyl)-2 phenyl-2 dioxasilacyclopentane-1,3,2

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) Et₂O, hexane, rt, 48 h, 2.) rt, 48 h

2: 87 percent / CCl₄ / 15 h / 77 °C

With n-butyllithium; In tetrachloromethane;
DOI:10.1016/0022-328X(90)80080-J