5-(4-methoxy-2-methylphenyl) picolinate

Base Information

Chemical Name:5-(4-methoxy-2-methylphenyl) picolinate
CAS No.:1580504-31-9
Molecular Formula:C₁₅H₁₅NO₃
Molecular Weight:257.289
Hs Code.:

Synonyms:5-(4-methoxy-2-methylphenyl) picolinate

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Chemical Property of 5-(4-methoxy-2-methylphenyl) picolinate

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Technology Process of 5-(4-methoxy-2-methylphenyl) picolinate

There total 1 articles about 5-(4-methoxy-2-methylphenyl) picolinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.8%

: 29682-15-3
methyl 5-bromopicolinate

: 208399-66-0
4-methoxy-2-methylphenyl boronic acid

: 1580504-31-9
5-(4-methoxy-2-methylphenyl) picolinate

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; cesium fluoride; In methanol; at 120 ℃; for 0.5h; Inert atmosphere; Microwave irradiation;
DOI:10.1021/ml4004815

Reference yield: 67.3%

: 1580504-31-9
5-(4-methoxy-2-methylphenyl) picolinate

: 1580504-32-0
5-((4-methoxy-2-methylphenyl)pyridin-2-yl)methanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ml4004815

Reference yield:

: 1580504-31-9
5-(4-methoxy-2-methylphenyl) picolinate

: 1580504-34-2
2-((5-(4-methoxy-2-methylphenyl)pyridin-2-yl)methoxy)nicotinamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

2.1: sodium hydride / paraffin oil; N,N-dimethyl-formamide / 0.67 h / 0 - 20 °C / Inert atmosphere

2.2: 2.17 h / 0 - 100 °C / Inert atmosphere

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; paraffin oil;
DOI:10.1021/ml4004815