C₁₂H₈Br₃N₇O₂

Base Information

Chemical Name:C₁₂H₈Br₃N₇O₂
CAS No.:1346427-59-5
Molecular Formula:C₁₂H₈Br₃N₇O₂
Molecular Weight:521.953
Hs Code.:

C<sub>12</sub>H<sub>8</sub>Br<sub>3</sub>N<sub>7</sub>O<sub>2</sub>

Synonyms:C₁₂H₈Br₃N₇O₂

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Chemical Property of C₁₂H₈Br₃N₇O₂

Chemical Property:

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Technology Process of C₁₂H₈Br₃N₇O₂

There total 9 articles about C₁₂H₈Br₃N₇O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63516-03-0
α-bromo-p-toluidine

: 1346427-59-5
C₁₂H₈Br₃N₇O₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: bromine; copper(ll) bromide / acetonitrile / 1 h / 50 °C

1.2: 0.5 h

2.1: sodium azide / N,N-dimethyl-formamide

3.1: sodium hydroxide / ethanol / 3 h / 85 °C

4.1: tert.-butylnitrite / tetrahydrofuran / 3 h / 50 °C

5.1: triethylamine; trifluoroacetic anhydride / dichloromethane / 2 h / 20 °C

6.1: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 2 h / 105 °C

7.1: triethylamine / tetrahydrofuran / 2 h / Reflux

8.1: methanol; sodium hydroxide / tetrahydrofuran / 3 h / 20 °C

With methanol; sodium azide; tert.-butylnitrite; bromine; ammonium chloride; triethylamine; trifluoroacetic anhydride; sodium hydroxide; copper(ll) bromide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmcl.2011.08.073

Reference yield:

: C₁₄H₁₂Br₃N₇O₂

: 1346427-59-5
C₁₂H₈Br₃N₇O₂

Guidance literature:: With methanol; sodium hydroxide; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1016/j.bmcl.2011.08.073

Reference yield:

: 1213234-82-2
3,4,5-tribromobenzyl azide

: 1346427-59-5
C₁₂H₈Br₃N₇O₂

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydroxide / ethanol / 3 h / 85 °C

2: tert.-butylnitrite / tetrahydrofuran / 3 h / 50 °C

3: triethylamine; trifluoroacetic anhydride / dichloromethane / 2 h / 20 °C

4: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 2 h / 105 °C

5: triethylamine / tetrahydrofuran / 2 h / Reflux

6: methanol; sodium hydroxide / tetrahydrofuran / 3 h / 20 °C

With methanol; sodium azide; tert.-butylnitrite; ammonium chloride; triethylamine; trifluoroacetic anhydride; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.08.073