4-methoxyphenyl 4,6-O-benzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbamoyl)-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranosyl-(1->3)-6-O-acetyl-2-O-benzoyl-β-D-galactopyranoside

Base Information

Chemical Name:4-methoxyphenyl 4,6-O-benzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbamoyl)-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranosyl-(1->3)-6-O-acetyl-2-O-benzoyl-β-D-galactopyranoside
CAS No.:1374563-96-8
Molecular Formula:C₄₁H₄₁Cl₆NO₁₇
Molecular Weight:1032.49
Hs Code.:

4-methoxyphenyl 4,6-O-benzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbamoyl)-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranosyl-(1->3)-6-O-acetyl-2-O-benzoyl-β-D-galactopyranoside

Synonyms:4-methoxyphenyl 4,6-O-benzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbamoyl)-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranosyl-(1->3)-6-O-acetyl-2-O-benzoyl-β-D-galactopyranoside

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Chemical Property of 4-methoxyphenyl 4,6-O-benzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbamoyl)-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranosyl-(1->3)-6-O-acetyl-2-O-benzoyl-β-D-galactopyranoside

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Technology Process of 4-methoxyphenyl 4,6-O-benzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbamoyl)-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranosyl-(1->3)-6-O-acetyl-2-O-benzoyl-β-D-galactopyranoside

There total 4 articles about 4-methoxyphenyl 4,6-O-benzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbamoyl)-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranosyl-(1->3)-6-O-acetyl-2-O-benzoyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1374563-94-6
4-methoxyphenyl 4,6-O-benzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbamoyl)-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranosyl-(1->3)-2-O-benzoyl-β-D-galactopyranoside

: 108-24-7
acetic anhydride

: 1374563-96-8
4-methoxyphenyl 4,6-O-benzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbamoyl)-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranosyl-(1->3)-6-O-acetyl-2-O-benzoyl-β-D-galactopyranoside

Guidance literature:: With pyridine; In tetrahydrofuran; at 20 ℃; for 150h; Inert atmosphere;
DOI:10.1002/asia.201100928

Reference yield:

: 1268156-74-6
C₂₅H₂₃Cl₆NO₈S

: 1374563-96-8
4-methoxyphenyl 4,6-O-benzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbamoyl)-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranosyl-(1->3)-6-O-acetyl-2-O-benzoyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / 1 h / -20 °C / Molecular sieve; Inert atmosphere

2: tri-n-butylamine hydrofluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

3: pyridine / tetrahydrofuran / 150 h / 20 °C / Inert atmosphere

With pyridine; N-iodo-succinimide; trifluorormethanesulfonic acid; tri-n-butylamine hydrofluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1002/asia.201100928

Reference yield:

: 904684-04-4
4-methoxyphenyl 2-O-benzoyl-4,6-O-di-tert-butylsilylene-β-D-galactopyranoside

: 1374563-96-8
4-methoxyphenyl 4,6-O-benzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbamoyl)-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranosyl-(1->3)-6-O-acetyl-2-O-benzoyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / 1 h / -20 °C / Molecular sieve; Inert atmosphere

2: tri-n-butylamine hydrofluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

3: pyridine / tetrahydrofuran / 150 h / 20 °C / Inert atmosphere

With pyridine; N-iodo-succinimide; trifluorormethanesulfonic acid; tri-n-butylamine hydrofluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1002/asia.201100928