Phosphoric acid (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-3-hydroxy-tetrahydro-furan-2-ylmethyl ester 1-methyl-2-oxo-propyl ester

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Chemical Name:Phosphoric acid (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-3-hydroxy-tetrahydro-furan-2-ylmethyl ester 1-methyl-2-oxo-propyl ester
CAS No.:87471-45-2
Molecular Formula:C₃₆H₃₉N₆O₁₃P
Molecular Weight:794.712
Hs Code.:

Phosphoric acid (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-3-hydroxy-tetrahydro-furan-2-ylmethyl ester 1-methyl-2-oxo-propyl ester

Synonyms:Phosphoric acid (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-3-hydroxy-tetrahydro-furan-2-ylmethyl ester 1-methyl-2-oxo-propyl ester

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Chemical Property of Phosphoric acid (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-3-hydroxy-tetrahydro-furan-2-ylmethyl ester 1-methyl-2-oxo-propyl ester

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Technology Process of Phosphoric acid (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-3-hydroxy-tetrahydro-furan-2-ylmethyl ester 1-methyl-2-oxo-propyl ester

There total 3 articles about Phosphoric acid (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-3-hydroxy-tetrahydro-furan-2-ylmethyl ester 1-methyl-2-oxo-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 87471-36-1
C₅₆H₅₅N₆O₁₄P

: 87471-45-2
Phosphoric acid (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-3-hydroxy-tetrahydro-furan-2-ylmethyl ester 1-methyl-2-oxo-propyl ester

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 0.333333h;
DOI:10.1016/S0040-4020(01)91932-5

Reference yield:

: 60920-99-2
N⁴-Benzoyl-5'-O-monomethoxytrityl-2'-deoxycytidine

: 87471-45-2
Phosphoric acid (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-3-hydroxy-tetrahydro-furan-2-ylmethyl ester 1-methyl-2-oxo-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) triethylamine 2.) triethylamine / 1.) at 20 degC for 2 h, dichloromethane 2.) at 0 degC for 15 h, at 20 degC for 2 h., DMF

2: 86 percent / trifluoroacetic acid / CH₂Cl₂ / 0.33 h / 0 °C

With triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/S0040-4020(01)91932-5

Reference yield:

: 4836-13-9
N₄-benzoyl-2'-deoxycytidine

: 87471-45-2
Phosphoric acid (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-3-hydroxy-tetrahydro-furan-2-ylmethyl ester 1-methyl-2-oxo-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) triethylamine 2.) triethylamine / 1.) at 20 degC for 2 h, dichloromethane 2.) at 0 degC for 15 h, at 20 degC for 2 h., DMF

2: 86 percent / trifluoroacetic acid / CH₂Cl₂ / 0.33 h / 0 °C

With triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/S0040-4020(01)91932-5