(3S,4S)-trans-3-mercapto-4-(4-phenoxybenzenesulfonamido)pyrrolidine hydrochloride

Base Information

Chemical Name:(3S,4S)-trans-3-mercapto-4-(4-phenoxybenzenesulfonamido)pyrrolidine hydrochloride
CAS No.:1214272-27-1
Molecular Formula:C₁₆H₁₈N₂O₃S₂*ClH
Molecular Weight:386.923
Hs Code.:

Synonyms:(3S,4S)-trans-3-mercapto-4-(4-phenoxybenzenesulfonamido)pyrrolidine hydrochloride

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Chemical Property of (3S,4S)-trans-3-mercapto-4-(4-phenoxybenzenesulfonamido)pyrrolidine hydrochloride

Chemical Property:

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Technology Process of (3S,4S)-trans-3-mercapto-4-(4-phenoxybenzenesulfonamido)pyrrolidine hydrochloride

There total 4 articles about (3S,4S)-trans-3-mercapto-4-(4-phenoxybenzenesulfonamido)pyrrolidine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1214272-57-7
(3S,4S)-trans-N-Boc-3-mercapto-4-(4-phenoxybenzenesulfonamido)pyrrolidine

: 1214272-27-1
(3S,4S)-trans-3-mercapto-4-(4-phenoxybenzenesulfonamido)pyrrolidine hydrochloride

Guidance literature:: With hydrogenchloride; acetic acid; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jm400529f

Reference yield:

: 1214272-56-6
(3S,4S)-trans-N-Boc-3-acetylthio-4-(4-phenoxybenzenesulfonamido)pyrrolidine

: 1214272-27-1
(3S,4S)-trans-3-mercapto-4-(4-phenoxybenzenesulfonamido)pyrrolidine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: water; methylamine / methanol / 0.17 h / Inert atmosphere

2: hydrogenchloride; acetic acid / 1 h / 20 °C

With hydrogenchloride; water; acetic acid; methylamine; In methanol;

Reference yield:

: 1214272-55-5
(3R,4S)-cis-N-Boc-3-hydroxy-4-(4-phenoxybenzenesulfonamido)pyrrolidine

: 1214272-27-1
(3S,4S)-trans-3-mercapto-4-(4-phenoxybenzenesulfonamido)pyrrolidine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 6 h / 20 °C

2: water; methylamine / methanol / 0.17 h / Inert atmosphere

3: hydrogenchloride; acetic acid / 1 h / 20 °C

With hydrogenchloride; water; acetic acid; triphenylphosphine; methylamine; diethylazodicarboxylate; In tetrahydrofuran; methanol;