[Fe(CO)₄(PCy₃)]

Base Information

Chemical Name:[Fe(CO)₄(PCy₃)]
CAS No.:18474-81-2
Molecular Formula:C₂₂H₃₃FeO₄P
Molecular Weight:448.322
Hs Code.:

Synonyms:[Fe(CO)₄(PCy₃)]

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Chemical Property of [Fe(CO)₄(PCy₃)]

Chemical Property:

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Technology Process of [Fe(CO)₄(PCy₃)]

There total 5 articles about [Fe(CO)₄(PCy₃)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 13463-40-6,37220-42-1
iron pentacarbonyl

: 2622-14-2
tricyclohexylphosphine

: 18474-81-2
[Fe(CO)₄(PCy₃)]

Guidance literature:: [(η(5)-C5H4Me)Fe(CO)2]2; In toluene; to boiling soln. of Fe(CO)5 and catalyst added ligand, heated for 3.5 h; evapd. in vac., chromd., recrystd.;
DOI:10.1016/S0022-328X(00)89069-5

Reference yield:

: Fe₂(CO)5(C₁₀H₈N₂)(P(C₄H₉)3)P(C₆H₁₁)3

: 18474-81-2
[Fe(CO)₄(PCy₃)]

: 114024-74-7
Fe(CO)2(C₁₀H₈N₂)(P(C₄H₉)3)

Guidance literature:: In further solvent(s); Heating of complex soln. in 2-Me-THF from 133°K to above 200°K, mechanism of decompn. discussed.;
DOI:10.1016/0022-328X(88)80078-0

Reference yield:

: 177174-06-0
Fe(CO)4(C(O)OCH₃)(C(O)C(O)CH₃)

: 2622-14-2
tricyclohexylphosphine

: 18474-81-2
[Fe(CO)₄(PCy₃)]

: 25921-51-1,40697-14-1
[Fe(CO)₃(PCy₃)₂]

: 177174-08-2
[Fe(CO)4(C(O)OC(Me)(OMe)C(O))]

: 1096549-85-7
Fe(CO)3(C(O)OCH₃)(C(O)C(O)CH₃)(P(C₆H₁₁)3)

Guidance literature:: In dichloromethane; under Ar; phosphine added with stirring to soln. of Fe complex in CH2Cl2at -20°C; temp. raised to 10°C; stirred for 24 h; solvent evapd.; extd. with hexanes-CH2Cl2 at 0°C; solvent removed; detd. by NMR spectra;
DOI:10.1021/om800804b