Re(C₅H₅)(P(C₆H₅)3)(NO)(CH₂CH₂C₆H₅)

Base Information

Chemical Name:Re(C₅H₅)(P(C₆H₅)3)(NO)(CH₂CH₂C₆H₅)
CAS No.:85926-75-6
Molecular Formula:C₃₁H₂₉NOPRe
Molecular Weight:648.758
Hs Code.:

Re(C<sub>5</sub>H<sub>5</sub>)(P(C<sub>6</sub>H<sub>5</sub>)3)(NO)(CH<sub>2</sub>CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)

Synonyms:Re(C₅H₅)(P(C₆H₅)3)(NO)(CH₂CH₂C₆H₅)

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Chemical Property of Re(C₅H₅)(P(C₆H₅)3)(NO)(CH₂CH₂C₆H₅)

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Technology Process of Re(C₅H₅)(P(C₆H₅)3)(NO)(CH₂CH₂C₆H₅)

There total 2 articles about Re(C₅H₅)(P(C₆H₅)3)(NO)(CH₂CH₂C₆H₅) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 82582-48-7
(η-C5H5)Re(NO)(PPh3)(COCH2C6H5)

: Tetrahydro-furan; compound with trifluoroborane

: 85926-75-6
Re(C₅H₅)(P(C₆H₅)3)(NO)(CH₂CH₂C₆H₅)

Guidance literature:: In tetrahydrofuran; to a 25°C soln. of Re-complex in THF was added BF3*THF in THF, refluxed for 4.5 h; evapd., extd. with C6H6, filtered through silica gel, evapd., chromd. (silica gel, CH2Cl2/hexanes);
DOI:10.1021/ja00353a020

Reference yield: 20.0%

: 71763-23-0
[(η(5)-cyclopentadienyl)Re(NO)(P(C6H5)3)(methylidene)]PF6

: 6921-34-2
benzylmagnesium chloride

: 85926-75-6
Re(C₅H₅)(P(C₆H₅)3)(NO)(CH₂CH₂C₆H₅)

Guidance literature:: In tetrahydrofuran; dichloromethane; to CH2Cl2 at -78°C was added Re-complex, C6H5CH2MgCl was added in THF, stood for 15 min, warmed to room temp.; evapd., the residue was taken in CH2Cl2/C6H6, filtered through silica gel, evapd., chromd. (silica gel, CH2Cl2/hexanes);
DOI:10.1021/ja00353a020