2-Oxazolidinone,5-ethenyl-5-methyl-4-(1-methylethyl)-,(4S)-(9CI)

Base Information

Chemical Name:2-Oxazolidinone,5-ethenyl-5-methyl-4-(1-methylethyl)-,(4S)-(9CI)
CAS No.:265996-24-5
Molecular Formula:C₉H₁₅NO₂
Molecular Weight:169.224
Hs Code.:
Mol file:265996-24-5.mol

Synonyms:2-Oxazolidinone,5-ethenyl-5-methyl-4-(1-methylethyl)-,(4S)-(9CI)

Suppliers and Price of 2-Oxazolidinone,5-ethenyl-5-methyl-4-(1-methylethyl)-,(4S)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-Oxazolidinone,5-ethenyl-5-methyl-4-(1-methylethyl)-,(4S)-(9CI)

Chemical Property:

PSA：38.33000
LogP:2.02430

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Oxazolidinone,5-ethenyl-5-methyl-4-(1-methylethyl)-,(4S)-(9CI)

There total 3 articles about 2-Oxazolidinone,5-ethenyl-5-methyl-4-(1-methylethyl)-,(4S)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 265996-15-4
(4S)-4-N-(tert-butyloxycarbonyl)amino-3-hydroxy-3,5-dimethylhex-1-ene

: 265996-24-5
(4S)-5-ethenyl-4-(2-propyl)-5-methyloxazolidin-2-one

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃; for 21h;
DOI:10.1021/ja993897c

Reference yield:

: N-(tert-butoxycarbonyl)valine methoxymethylamide

: 265996-24-5
(4S)-5-ethenyl-4-(2-propyl)-5-methyloxazolidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether; tetrahydrofuran / 2 h / 0 °C

2: 40 percent / tetrahydrofuran / 2 h / 20 °C

3: 75 percent / NaH / tetrahydrofuran; various solvent(s) / 21 h / 20 °C

With sodium hydride; In tetrahydrofuran; diethyl ether; 1: Grignard reaction / 2: Addition / 3: Cyclization;
DOI:10.1021/ja993897c

Reference yield:

: 128211-52-9,327600-47-5
(3S)-3-N-(tert-butyloxycarbonyl)amino-4-methylpentan-2-one

: 265996-24-5
(4S)-5-ethenyl-4-(2-propyl)-5-methyloxazolidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / tetrahydrofuran / 2 h / 20 °C

2: 75 percent / NaH / tetrahydrofuran; various solvent(s) / 21 h / 20 °C

With sodium hydride; In tetrahydrofuran; 1: Addition / 2: Cyclization;
DOI:10.1021/ja993897c