(S)-2-phthalimido-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-3-(p-tolyl)propanamide

Base Information

Chemical Name:(S)-2-phthalimido-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-3-(p-tolyl)propanamide
CAS No.:1582806-67-4
Molecular Formula:C₂₅H₁₅F₇N₂O₃
Molecular Weight:524.395
Hs Code.:

Synonyms:(S)-2-phthalimido-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-3-(p-tolyl)propanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-phthalimido-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-3-(p-tolyl)propanamide

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Technology Process of (S)-2-phthalimido-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-3-(p-tolyl)propanamide

There total 7 articles about (S)-2-phthalimido-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-3-(p-tolyl)propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 624-31-7
4-tolyl iodide

: 1582806-46-9
(S)-2-phthalimido-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)propanamide

: 1582806-67-4
(S)-2-phthalimido-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-3-(p-tolyl)propanamide

Guidance literature:: With α-picoline; palladium(II) trifluoroacetate; silver carbonate; trifluoroacetic acid; In 1,2-dichloro-ethane; at 100 ℃; for 20h;
DOI:10.1126/science.1249198

Reference yield: 83.0%

: 1582806-46-9
(S)-2-phthalimido-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)propanamide

: 18412-57-2
p-tolyltriethoxysilane

: 1582806-67-4
(S)-2-phthalimido-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-3-(p-tolyl)propanamide

Guidance literature:: With palladium diacetate; silver fluoride; 8,9,10,11-tetrahydro-7H-cyclohepta[c]quinoline; In 1,4-dioxane; at 20 - 110 ℃; for 18h; Sealed tube;
DOI:10.1021/jacs.5b00890

Reference yield:

: 624-31-7
4-tolyl iodide

: 1582806-46-9
(S)-2-phthalimido-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)propanamide

: 1582806-67-4
(S)-2-phthalimido-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-3-(p-tolyl)propanamide

: C₃₂H₂₁F₇N₂O₃

Guidance literature:: With palladium(II) trifluoroacetate; silver carbonate; trifluoroacetic acid; In cyclohexane; at 100 ℃; for 20h; Overall yield = 94 %Spectr.; Sealed tube;
DOI:10.1002/adsc.201700707