chloro(triphenylphosphine sulfide)gold(I)

Base Information

Chemical Name:chloro(triphenylphosphine sulfide)gold(I)
CAS No.:15279-72-8
Molecular Formula:C₁₈H₁₅AuClPS
Molecular Weight:526.776
Hs Code.:

Synonyms:chloro(triphenylphosphine sulfide)gold(I)

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Chemical Property of chloro(triphenylphosphine sulfide)gold(I)

Chemical Property:

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Technology Process of chloro(triphenylphosphine sulfide)gold(I)

There total 2 articles about chloro(triphenylphosphine sulfide)gold(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 29892-37-3
chloro(dimethylsulfide) gold(I)

: 3878-45-3
triphenylphosphine sulfide

: 15279-72-8
chloro(triphenylphosphine sulfide)gold(I)

Guidance literature:: In dichloromethane; excess Ph3PS; concn. (vac.), Et2O addn., crystn. on cooling (refrigerator, overnight),filtration, washing (Et2O), drying (vac.); second crop from filtrate; e lem. anal.;
DOI:10.1039/DT9770001430

Reference yield:

: chloroauric acid

: 3878-45-3
triphenylphosphine sulfide

: 15279-72-8
chloro(triphenylphosphine sulfide)gold(I)

Guidance literature:: In ethanol; stirred a slight excess over the equimolar ratio of solid (C6H5)3PS with an ethanolic soln. of HAuCl4 for several h under N2 atmosphere; a soln. was leaving in the refrigerator for several days, sepd. the crystals;

Reference yield: 77.0%

: 23810-63-1
1,2-dicarba-closo-dodecaborane-1,2-dithiol

: 15279-72-8
chloro(triphenylphosphine sulfide)gold(I)

: 185520-02-9
[Au2(μ-1,2-dithiolate-o-carborane)(SPPh3)2]

Guidance literature:: With Na₂CO₃; In dichloromethane; 2 equiv. Au-complex, excess Na2CO3, stirring for 30 min; filtration, concn., pptn. on Et2O addn.; elem. anal.;