C₂₄H₂₅FN₂O₇S

Base Information

Chemical Name:C₂₄H₂₅FN₂O₇S
CAS No.:1374234-29-3
Molecular Formula:C₂₄H₂₅FN₂O₇S
Molecular Weight:504.536
Hs Code.:

C<sub>24</sub>H<sub>25</sub>FN<sub>2</sub>O<sub>7</sub>S

Synonyms:C₂₄H₂₅FN₂O₇S

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Chemical Property of C₂₄H₂₅FN₂O₇S

Chemical Property:

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Technology Process of C₂₄H₂₅FN₂O₇S

There total 8 articles about C₂₄H₂₅FN₂O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1374234-28-2
C₂₆H₂₉FN₂O₇S

: 1374234-29-3
C₂₄H₂₅FN₂O₇S

Guidance literature:: C₂₆H₂₉FN₂O₇S; With lithium hydroxide monohydrate; water; In tetrahydrofuran; ethanol; at 70 ℃; for 2h;

With hydrogenchloride; In tetrahydrofuran; ethanol; water; pH=3;

Reference yield:

: 691857-46-2
ethyl 2-(4-fluorophenyl)-5-hydroxy-6-nitrobenzofuran-3-carboxylate

: 1374234-29-3
C₂₄H₂₅FN₂O₇S

Guidance literature:: Multi-step reaction with 7 steps

1.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 2 h / 0 °C

2.1: triethylamine / bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / 1 h / 20 °C / Inert atmosphere

3.1: pyridine / dmap / dichloromethane / 2 h / 0 - 20 °C

4.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 20 °C

5.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / Reflux

6.1: dichloromethane / 2 h / 0 - 20 °C

6.2: 3 h / 0 - 20 °C

7.1: lithium hydroxide monohydrate; water / tetrahydrofuran; ethanol / 2 h / 70 °C

7.2: pH 3

With pyridine; lithium hydroxide monohydrate; water; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate;

Reference yield:

: 691857-07-5
ethyl 2-(4-fluorophenyl)-5-isopropoxy-6-nitrobenzofuran-3-carboxylate

: 1374234-29-3
C₂₄H₂₅FN₂O₇S

Guidance literature:: Multi-step reaction with 8 steps

1.1: boron trichloride / dichloromethane / 1 h / 0 - 20 °C

1.2: Cooling with ice

2.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 2 h / 0 °C

3.1: triethylamine / bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / 1 h / 20 °C / Inert atmosphere

4.1: pyridine / dmap / dichloromethane / 2 h / 0 - 20 °C

5.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 20 °C

6.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / Reflux

7.1: dichloromethane / 2 h / 0 - 20 °C

7.2: 3 h / 0 - 20 °C

8.1: lithium hydroxide monohydrate; water / tetrahydrofuran; ethanol / 2 h / 70 °C

8.2: pH 3

With pyridine; lithium hydroxide monohydrate; water; hydrogen; boron trichloride; triethylamine; N-ethyl-N,N-diisopropylamine; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate;