trans-(benzoic acid-C₃)(isonicotinic acid)bis(triphenylphosphine)platinum(II) triflate

Base Information

• Chemical Name: trans-(benzoic acid-C₃)(isonicotinic acid)bis(triphenylphosphine)platinum(II) triflate
• CAS No.: 360048-36-8
• Molecular Formula: CF₃O₃S*C₄₉H₄₀NO₄P₂Pt
• Molecular Weight: 1112.96

Synonyms:trans-(benzoic acid-C₃)(isonicotinic acid)bis(triphenylphosphine)platinum(II) triflate

Chemical Property of trans-(benzoic acid-C₃)(isonicotinic acid)bis(triphenylphosphine)platinum(II) triflate

Chemical Property:

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Technology Process of trans-(benzoic acid-C₃)(isonicotinic acid)bis(triphenylphosphine)platinum(II) triflate

There total 2 articles about trans-(benzoic acid-C₃)(isonicotinic acid)bis(triphenylphosphine)platinum(II) triflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

trans-(isonicotinic acid)(tert-butyldiphenylsilyl benzoate-C3)bis(triphenylphosphine)platinum(II) triflate (360048-28-8) → trans-(benzoic acid-C3)(isonicotinic acid)bis(triphenylphosphine)platinum(II) triflate (360048-36-8)

Guidance literature:

With CF₃SO₃H; In dichloromethane; to a stirred soln. of complex in CH2Cl2 was added CF3SO3H, the mixt. wasstirred at room temp. for 2 h (N2); diethyl ether was added, ppt. was filtered off, washed with diethyl ether, dried in vac., recrystd. from CH2Cl2/diethyl ether; elem. anal.;

DOI:10.1021/om010127c

Reference yield:

pyridine-4-carboxylic acid (55-22-1) + trans-iodo(tert-butyldiphenylsilylbenzoate-C(3))bis(triphenylphosphine)platinum(II) (360048-21-1) → trans-(benzoic acid-C3)(isonicotinic acid)bis(triphenylphosphine)platinum(II) triflate (360048-36-8)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane

2: CF₃SO₃H / dichloromethane

With CF₃SO₃H; In dichloromethane;

DOI:10.1021/om010127c

upstream raw materials:

trans-(isonicotinic acid)(tert-butyldiphenylsilyl benzoate-C₃)bis(triphenylphosphine)platinum(II) triflate

pyridine-4-carboxylic acid

trans-iodo(tert-butyldiphenylsilylbenzoate-C⁽³⁾)bis(triphenylphosphine)platinum(II)

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