Technology Process of N-methyl-2,4,6-trimethyldiphenylamine
There total 8 articles about N-methyl-2,4,6-trimethyldiphenylamine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-bromomesitylene;
With
PdCl(cinnamyl)(N,N′-bis(2,6-bis(diphenylmethyl)-4-methylphenyl)imidazol-2-ylidene); potassium 2-methylbutan-2-olate;
In
neat (no solvent);
at 25 ℃;
for 0.0833333h;
N-methylaniline;
In
neat (no solvent);
at 25 ℃;
for 24h;
DOI:10.1039/c3ra40386f
- Guidance literature:
-
With
sodium hydride;
In
1-methyl-pyrrolidin-2-one; mineral oil;
at 100 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 2.9 percent / K2CO3, Cu / nitrobenzene / 48 h / 200 °C
2: 70 percent / KOH / various solvent(s) / 24 h / Heating
3: 2.) NaOH / 1.) 200 deg C, 3 h, 2.) reflux, 2.5 h
With
potassium hydroxide; sodium hydroxide; copper; potassium carbonate;
In
nitrobenzene;
DOI:10.1021/ja00413a019
