tert-butyl 2-(2-hydroxy-5-(1,1-dioxidothiomorpholin-4-yl)benzamido)-4-phenylbenzoate

Base Information

Chemical Name:tert-butyl 2-(2-hydroxy-5-(1,1-dioxidothiomorpholin-4-yl)benzamido)-4-phenylbenzoate
CAS No.:1237519-61-7
Molecular Formula:C₂₈H₃₀N₂O₆S
Molecular Weight:522.622
Hs Code.:

Synonyms:tert-butyl 2-(2-hydroxy-5-(1,1-dioxidothiomorpholin-4-yl)benzamido)-4-phenylbenzoate

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Chemical Property of tert-butyl 2-(2-hydroxy-5-(1,1-dioxidothiomorpholin-4-yl)benzamido)-4-phenylbenzoate

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Technology Process of tert-butyl 2-(2-hydroxy-5-(1,1-dioxidothiomorpholin-4-yl)benzamido)-4-phenylbenzoate

There total 3 articles about tert-butyl 2-(2-hydroxy-5-(1,1-dioxidothiomorpholin-4-yl)benzamido)-4-phenylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1237519-60-6
tert-butyl 2-(2-(benzyloxy)-5-(1,1,4-trioxidothiomorpholin-4-yl)benzamido)-4-phenylbenzoate

: 1237519-61-7
tert-butyl 2-(2-hydroxy-5-(1,1-dioxidothiomorpholin-4-yl)benzamido)-4-phenylbenzoate

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In methanol; ethyl acetate; at 20 ℃; for 2.5h;

Reference yield:

: 1237515-25-1
tert-butyl 2-(2-(benzyloxy)-5-(thiomorpholin-4-yl)benzamido)-4-phenylbenzoate

: 1237519-61-7
tert-butyl 2-(2-hydroxy-5-(1,1-dioxidothiomorpholin-4-yl)benzamido)-4-phenylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C / Cooling with ice

2: hydrogen / palladium 10% on activated carbon / ethyl acetate; methanol / 2.5 h / 20 °C

With hydrogen; 3-chloro-benzenecarboperoxoic acid; palladium 10% on activated carbon; In methanol; dichloromethane; ethyl acetate;

Reference yield:

: 1237514-90-7
tert-butyl 2-(2-(benzyloxy)-5-bromobenzamido)-4-phenylbenzoate

: 1237519-61-7
tert-butyl 2-(2-hydroxy-5-(1,1-dioxidothiomorpholin-4-yl)benzamido)-4-phenylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / bis(dibenzylideneacetone)-palladium⁽⁰⁾; XPhos / toluene / 5 h / Reflux; Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C / Cooling with ice

3: hydrogen / palladium 10% on activated carbon / ethyl acetate; methanol / 2.5 h / 20 °C

With hydrogen; caesium carbonate; 3-chloro-benzenecarboperoxoic acid; palladium 10% on activated carbon; bis(dibenzylideneacetone)-palladium⁽⁰⁾; XPhos; In methanol; dichloromethane; ethyl acetate; toluene;