5-acetylbrevifoliol

Base Information

• Chemical Name: 5-acetylbrevifoliol
• CAS No.: 708212-67-3
• Molecular Formula: C₃₃H₄₂O₁₀
• Molecular Weight: 598.69
• Mol file: 708212-67-3.mol

Synonyms:5-acetylbrevifoliol

Chemical Property of 5-acetylbrevifoliol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 5-acetylbrevifoliol

There total 2 articles about 5-acetylbrevifoliol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

acetic anhydride (108-24-7) + brevifoliol (134955-83-2) → 5-acetylbrevifoliol (708212-67-3) + 10β-benzoxy-1β,5α-dihydroxy-7β,9α,13α-triacetoxy-11(15->1)-abeotaxa-4(20),11-diene (153229-35-7)

Guidance literature:

With pyridine; 3 A molecular sieve; at 20 ℃; for 20h;

DOI:10.1021/np0304565

Reference yield: 45.0%

5-acetyl-13-oxobrevifoliol (708212-71-9) → 5-acetylbrevifoliol (708212-67-3)

Guidance literature:

With sodium tetrahydroborate; In ethanol; at 25 ℃; for 3h;

DOI:10.1021/np0304565

Reference yield: 78.0%

5-acetylbrevifoliol (708212-67-3) → 5-acetyl-13-oxobrevifoliol (708212-71-9)

Guidance literature:

With pyridinium chlorochromate; In dichloromethane; for 16h;

DOI:10.1021/np0304565

upstream raw materials:

5-acetyl-13-oxobrevifoliol

acetic anhydride

brevifoliol

Downstream raw materials:

5α-acetyl-13α-[(2'S)-O-(tetrahydropyran-2-yl)-3-phenyllactate]brevifoliol

5-acetyl-13-oxobrevifoliol