N-(6-(3-ethynylphenoxy)hexyl)-2,3,4,6-tetra-O-acetyl-1,5-dideoxy-1,5-imino-D-glucitol

Base Information

Chemical Name:N-(6-(3-ethynylphenoxy)hexyl)-2,3,4,6-tetra-O-acetyl-1,5-dideoxy-1,5-imino-D-glucitol
CAS No.:1017579-84-8
Molecular Formula:C₂₈H₃₇NO₉
Molecular Weight:531.603
Hs Code.:

Synonyms:N-(6-(3-ethynylphenoxy)hexyl)-2,3,4,6-tetra-O-acetyl-1,5-dideoxy-1,5-imino-D-glucitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(6-(3-ethynylphenoxy)hexyl)-2,3,4,6-tetra-O-acetyl-1,5-dideoxy-1,5-imino-D-glucitol

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Technology Process of N-(6-(3-ethynylphenoxy)hexyl)-2,3,4,6-tetra-O-acetyl-1,5-dideoxy-1,5-imino-D-glucitol

There total 1 articles about N-(6-(3-ethynylphenoxy)hexyl)-2,3,4,6-tetra-O-acetyl-1,5-dideoxy-1,5-imino-D-glucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1017579-81-5
N-(6-(3-ethynylphenoxy)hexyl)-1,5-dideoxy-1,5-imino-D-glucitol

: 108-24-7
acetic anhydride

: 1017579-84-8
N-(6-(3-ethynylphenoxy)hexyl)-2,3,4,6-tetra-O-acetyl-1,5-dideoxy-1,5-imino-D-glucitol

Guidance literature:: With pyridine; dmap;
DOI:10.1016/j.bmcl.2007.12.034

Reference yield: 100.0%

: 1017579-84-8
N-(6-(3-ethynylphenoxy)hexyl)-2,3,4,6-tetra-O-acetyl-1,5-dideoxy-1,5-imino-D-glucitol

: 1017579-71-3
C₂₀H₃₀N₄O₅

Guidance literature:: N-(6-(3-ethynylphenoxy)hexyl)-2,3,4,6-tetra-O-acetyl-1,5-dideoxy-1,5-imino-D-glucitol; With benzyl azide; In toluene; for 48h; Heating;

With sodium methylate; In methanol; at 20 ℃;

With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; Further stages.;
DOI:10.1016/j.bmc.2008.05.012

Reference yield:

: 1017579-84-8
N-(6-(3-ethynylphenoxy)hexyl)-2,3,4,6-tetra-O-acetyl-1,5-dideoxy-1,5-imino-D-glucitol

: 622-79-7
benzyl azide

: 1017579-71-3
C₂₀H₃₀N₄O₅

Guidance literature:: N-(6-(3-ethynylphenoxy)hexyl)-2,3,4,6-tetra-O-acetyl-1,5-dideoxy-1,5-imino-D-glucitol; benzyl azide; In toluene; for 48h; Heating;

With sodium methylate; In methanol;

With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; Further stages.;
DOI:10.1016/j.bmcl.2007.12.034