Technology Process of C42H42N8O6
There total 11 articles about C42H42N8O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
HATU;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 1.5h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: ammonium hydroxide / methanol; water / 20 °C
2: N-iodo-succinimide / dichloromethane / 1 h / 0 °C
3: water; sodium sulfite / ethanol / 17 h / Reflux
4: triethylamine / dmap / dichloromethane / 2 h / 20 °C
5: triethylamine / tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 1 h / 120 °C / Inert atmosphere; microwave irradiation
6: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C
7: HATU / N,N-dimethyl-formamide / 1.5 h / 20 °C
With
hydrogenchloride; ammonium hydroxide; N-iodo-succinimide; water; triethylamine; HATU; sodium sulfite;
dmap; tetrakis(triphenylphosphine) palladium(0);
In
1,4-dioxane; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: N-iodo-succinimide / dichloromethane / 1 h / 0 °C
2: water; sodium sulfite / ethanol / 17 h / Reflux
3: triethylamine / dmap / dichloromethane / 2 h / 20 °C
4: triethylamine / tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 1 h / 120 °C / Inert atmosphere; microwave irradiation
5: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C
6: HATU / N,N-dimethyl-formamide / 1.5 h / 20 °C
With
hydrogenchloride; N-iodo-succinimide; water; triethylamine; HATU; sodium sulfite;
dmap; tetrakis(triphenylphosphine) palladium(0);
In
1,4-dioxane; ethanol; dichloromethane; N,N-dimethyl-formamide;