Technology Process of C16H22O5S2
There total 3 articles about C16H22O5S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water; trifluoroacetic acid;
In
dichloromethane;
for 3h;
Heating;
DOI:10.1039/b606362b
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: LDA / tetrahydrofuran; hexane / 0.5 h / -78 °C
1.2: tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / 2 h / -78 - 0 °C
2.1: 98 percent / TFA; H2O / CH2Cl2 / 3 h / Heating
With
water; trifluoroacetic acid; lithium diisopropyl amide;
In
tetrahydrofuran; hexane; dichloromethane;
DOI:10.1039/b606362b
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: LDA / tetrahydrofuran; hexane / 0.5 h / -78 °C
1.2: tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / 2 h / -78 - 0 °C
2.1: 98 percent / TFA; H2O / CH2Cl2 / 3 h / Heating
With
water; trifluoroacetic acid; lithium diisopropyl amide;
In
tetrahydrofuran; hexane; dichloromethane;
DOI:10.1039/b606362b