Benzyl-{cyclohexyl-[4-isobutyl-1-(2-trimethylsilanyl-ethoxymethyl)-1H-imidazol-2-yl]-methyl}-amine

Base Information

Chemical Name:Benzyl-{cyclohexyl-[4-isobutyl-1-(2-trimethylsilanyl-ethoxymethyl)-1H-imidazol-2-yl]-methyl}-amine
CAS No.:107750-97-0
Molecular Formula:C₂₇H₄₅N₃OSi
Molecular Weight:455.759
Hs Code.:

Synonyms:Benzyl-{cyclohexyl-[4-isobutyl-1-(2-trimethylsilanyl-ethoxymethyl)-1H-imidazol-2-yl]-methyl}-amine

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Chemical Property of Benzyl-{cyclohexyl-[4-isobutyl-1-(2-trimethylsilanyl-ethoxymethyl)-1H-imidazol-2-yl]-methyl}-amine

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Technology Process of Benzyl-{cyclohexyl-[4-isobutyl-1-(2-trimethylsilanyl-ethoxymethyl)-1H-imidazol-2-yl]-methyl}-amine

There total 4 articles about Benzyl-{cyclohexyl-[4-isobutyl-1-(2-trimethylsilanyl-ethoxymethyl)-1H-imidazol-2-yl]-methyl}-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 130517-97-4
benzyl-cyclohexylmethylene-amine

: C₁₃H₂₅LiN₂OSi

: 107750-97-0
Benzyl-{cyclohexyl-[4-isobutyl-1-(2-trimethylsilanyl-ethoxymethyl)-1H-imidazol-2-yl]-methyl}-amine

Guidance literature:: With boron trifluoride diethyl etherate; In tetrahydrofuran; at -78 ℃;
DOI:10.1016/S0040-4039(00)84919-9

Reference yield:

: 61893-08-1
4-isobutylimidazole

: 107750-97-0
Benzyl-{cyclohexyl-[4-isobutyl-1-(2-trimethylsilanyl-ethoxymethyl)-1H-imidazol-2-yl]-methyl}-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) KH / 1.) THF

2: n-BuLi / tetrahydrofuran / -78 °C

3: 87 percent / BF₃*Et₂O / tetrahydrofuran / -78 °C

With n-butyllithium; boron trifluoride diethyl etherate; potassium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)84919-9

Reference yield:

: 76513-69-4
(2-trimethylethylsilylethoxy)methyl chloride

: 107750-97-0
Benzyl-{cyclohexyl-[4-isobutyl-1-(2-trimethylsilanyl-ethoxymethyl)-1H-imidazol-2-yl]-methyl}-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) KH / 1.) THF

2: n-BuLi / tetrahydrofuran / -78 °C

3: 87 percent / BF₃*Et₂O / tetrahydrofuran / -78 °C

With n-butyllithium; boron trifluoride diethyl etherate; potassium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)84919-9