N-hydroxy-N-(2,2,2-trimethylacetyl)-2-bromobenzenesulfonamide

Base Information

Chemical Name:N-hydroxy-N-(2,2,2-trimethylacetyl)-2-bromobenzenesulfonamide
CAS No.:1352414-90-4
Molecular Formula:C₁₁H₁₄BrNO₄S
Molecular Weight:336.206
Hs Code.:

Synonyms:N-hydroxy-N-(2,2,2-trimethylacetyl)-2-bromobenzenesulfonamide

Suppliers and Price of N-hydroxy-N-(2,2,2-trimethylacetyl)-2-bromobenzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of N-hydroxy-N-(2,2,2-trimethylacetyl)-2-bromobenzenesulfonamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-hydroxy-N-(2,2,2-trimethylacetyl)-2-bromobenzenesulfonamide

There total 6 articles about N-hydroxy-N-(2,2,2-trimethylacetyl)-2-bromobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₂₂BrNO₅S

: 1352414-90-4
N-hydroxy-N-(2,2,2-trimethylacetyl)-2-bromobenzenesulfonamide

Guidance literature:: With hydrogenchloride; In methanol; at 0 ℃;
DOI:10.1021/ol203016c

Reference yield:

: 2905-25-1
o-bromobenzenesulfonyl chloride

: 1352414-90-4
N-hydroxy-N-(2,2,2-trimethylacetyl)-2-bromobenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / tetrahydrofuran; methanol; water

2: triethylamine / dichloromethane / 0.5 h

3: hydrogenchloride / methanol / 0 °C

With hydrogenchloride; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/ol203016c

Reference yield:

: 2-bromo-N-hydroxybenzenesulfonamide

: 1352414-90-4
N-hydroxy-N-(2,2,2-trimethylacetyl)-2-bromobenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1,1,1,3,3,3-hexamethyl-disilazane / chloroform / 0.5 h / Reflux

2: triethylamine / dichloromethane / 0.5 h

3: citric acid / methanol

With triethylamine; 1,1,1,3,3,3-hexamethyl-disilazane; citric acid; In methanol; dichloromethane; chloroform;
DOI:10.1021/ol203016c